Carbamic acid, [3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-( pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3 ,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Carbamic acid, [3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-( pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3 ,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester
CAS No.:537049-10-8
Molecular Formula:C₄₂H₅₁Cl₂N₁₇O₂
Molecular Weight:896.886
Hs Code.:

Carbamic acid,
[3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-(
pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3
,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester

Synonyms:

Suppliers and Price of Carbamic acid, [3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-( pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3 ,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester

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Chemical Property of Carbamic acid, [3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-( pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3 ,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Carbamic acid, [3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-( pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3 ,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester

There total 8 articles about Carbamic acid, [3-[[4-[[3-[[4-[[3-[(4,6-dichloro-1,3,5-triazin-2-yl)amino]phenyl]amino]-6-( pentylamino)-1,3,5-triazin-2-yl]amino]phenyl]amino]-6-(pentylamino)-1,3 ,5-triazin-2-yl]amino]phenyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 68621-88-5
(3-aminophenyl)carbamic acid tert-butyl ester

: 537049-10-8
{3-[4-(3-{4-[3-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-phenylamino]-6-pentylamino-[1,3,5]triazin-2-ylamino}-phenylamino)-6-pentylamino-[1,3,5]triazin-2-ylamino]-phenyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 8 steps

1: 85 percent / NaHCO₃ / acetone; H₂O / 0 °C

2: 91 percent / NaHCO₃ / acetone; H₂O / 50 °C

3: 95 percent / tetrahydrofuran / 60 °C

4: TFA / CH₂Cl₂

5: 84 percent / NaHCO₃ / acetone; H₂O / 50 °C

6: 91 percent / tetrahydrofuran / 60 °C

7: H₂ / Pd/C / methanol / 3 h

8: acetone; H₂O / 2 h / 0 °C

With hydrogen; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1016/S0040-4039(02)02884-8

Reference yield:

: 537049-05-1
2-[3-(tert-butoxycarbonylamino)phenylamino]-4,6-dichloro-1,3,5-triazine

: 537049-10-8
{3-[4-(3-{4-[3-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-phenylamino]-6-pentylamino-[1,3,5]triazin-2-ylamino}-phenylamino)-6-pentylamino-[1,3,5]triazin-2-ylamino]-phenyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / NaHCO₃ / acetone; H₂O / 50 °C

2: 95 percent / tetrahydrofuran / 60 °C

3: TFA / CH₂Cl₂

4: 84 percent / NaHCO₃ / acetone; H₂O / 50 °C

5: 91 percent / tetrahydrofuran / 60 °C

6: H₂ / Pd/C / methanol / 3 h

7: acetone; H₂O / 2 h / 0 °C

With hydrogen; sodium hydrogencarbonate; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1016/S0040-4039(02)02884-8

Reference yield:

: {3-[4-(3-amino-phenylamino)-6-pentylamino-[1,3,5]triazin-2-ylamino]-phenyl}-carbamic acid benzyl ester

: 537049-10-8
{3-[4-(3-{4-[3-(4,6-dichloro-[1,3,5]triazin-2-ylamino)-phenylamino]-6-pentylamino-[1,3,5]triazin-2-ylamino}-phenylamino)-6-pentylamino-[1,3,5]triazin-2-ylamino]-phenyl}-carbamic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / NaHCO₃ / acetone; H₂O / 50 °C

2: 91 percent / tetrahydrofuran / 60 °C

3: H₂ / Pd/C / methanol / 3 h

4: acetone; H₂O / 2 h / 0 °C

With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In tetrahydrofuran; methanol; water; acetone;
DOI:10.1016/S0040-4039(02)02884-8