Technology Process of Benzoxazole, 2-[4-(bromomethyl)-3-methoxyphenyl]-
There total 3 articles about Benzoxazole, 2-[4-(bromomethyl)-3-methoxyphenyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide; dibenzoyl peroxide;
In
tetrachloromethane;
for 1h;
UV-irradiation;
heating;
DOI:10.1016/j.bmc.2003.10.021
- Guidance literature:
-
Multi-step reaction with 4 steps
1: thionyl chloride / 2 h / Heating
2: 100 percent / diisopropylethylamine / tetrahydrofuran / 0 - 20 °C
3: 50 percent / p-toluenesulfonic acid monohydrate / toluene / Heating
4: 100 percent / benzoyl peroxide; N-bromosuccinimide / CCl4 / 1 h / UV-irradiation; heating
With
N-Bromosuccinimide; thionyl chloride; toluene-4-sulfonic acid; N-ethyl-N,N-diisopropylamine; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; toluene;
DOI:10.1016/j.bmc.2003.10.021
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 50 percent / p-toluenesulfonic acid monohydrate / toluene / Heating
2: 100 percent / benzoyl peroxide; N-bromosuccinimide / CCl4 / 1 h / UV-irradiation; heating
With
N-Bromosuccinimide; toluene-4-sulfonic acid; dibenzoyl peroxide;
In
tetrachloromethane; toluene;
DOI:10.1016/j.bmc.2003.10.021
