2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine

Base Information

Chemical Name:2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine
CAS No.:54098-18-9
Molecular Formula:C₁₈H₂₀NP
Molecular Weight:281.337
Hs Code.:
DSSTox Substance ID:DTXSID10500309
Nikkaji Number:J2.193.988I
Wikidata:Q82351795

Synonyms:54098-18-9;2-(Diphenylphosphino)-N,N-diethylethynamine;2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine;DTXSID10500309

Suppliers and Price of 2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine

Chemical Property:

Boiling Point:387.0±25.0 °C(Predicted)
PSA：16.83000
LogP:3.37950
XLogP3:4.6
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:6
Exact Mass:281.133336640
Heavy Atom Count:20
Complexity:306

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C#CP(C1=CC=CC=C1)C2=CC=CC=C2

Technology Process of 2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine

There total 1 articles about 2-(Diphenylphosphanyl)-N,N-diethylethyn-1-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54098-18-9
2-(diethylamino)-1-(diphenylphosphanyl)acetylene

Guidance literature:: Chlordiphenylphosphin Ph2PCl, /BRN= 125679/;

Reference yield: 65.0%

: bis(η2-ethylene)(η5-pentamethylcyclopentadienyl)cobalt(I)

: 54098-18-9
2-(diethylamino)-1-(diphenylphosphanyl)acetylene

: ((C₅(CH₃)5)Co)2(N(C₂H₅)2C₂P(C₆H₅)2)

: 861659-32-7
(η5-pentamethylcyclopentadienyl)(η4-bis(diphenylphosphino)bis(diethylamino)cyclobutadiene)cobalt(I)

Guidance literature:: In hexane; N2 atm.; aminoacetylene and Co-complex were heated at 70°C in hexane for 2 d, cooled; filtered, the solvent was removed by high vac.; column chromy. on silicagel, hexane-toluene 1:1; as oil;
DOI:10.1016/j.jorganchem.2005.03.056

Reference yield: 58.0%

: 208046-85-9
carbonyl(η(5)-cyclopentadienyl)(η(2)-bis(tert-butylsulfonyl)acetylene)cobalt(I)

: 54098-18-9
2-(diethylamino)-1-(diphenylphosphanyl)acetylene

: 894493-98-2
[η4-1,2-bis(tert-butylsulfonyl)-4-diethylamino-3-diphenylphosphanylcyclobutadiene](η5-cyclopentadienyl)cobalt

Guidance literature:: In toluene; under N2, Schlenk techniques; 1:1 mixt. stirred at room temp. for 2 d; evapd., chromd. (silica, THF/toluene=2/1), recrystd. (toluene, -20°C), elem. anal.;
DOI:10.1002/ejic.200500308