3,5-BIS[(3-CHLOROPHENYL)METHYLENE]-1-METHYLTETRAHYDRO-4(1H)-PYRIDINONE

Base Information

Chemical Name:3,5-BIS[(3-CHLOROPHENYL)METHYLENE]-1-METHYLTETRAHYDRO-4(1H)-PYRIDINONE
CAS No.:54237-29-5
Molecular Formula:C20H17Cl2NO
Molecular Weight:358.26100
Hs Code.:
Mol file:54237-29-5.mol

Synonyms:3,5-Bis-[1-(3-chloro-phenyl)-meth-(E)-ylidene]-1-methyl-piperidin-4-one;

Suppliers and Price of 3,5-BIS[(3-CHLOROPHENYL)METHYLENE]-1-METHYLTETRAHYDRO-4(1H)-PYRIDINONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-BIS[(3-CHLOROPHENYL)METHYLENE]-1-METHYLTETRAHYDRO-4(1H)-PYRIDINONE

Chemical Property:

Melting Point:117 - 119 °C
PSA：20.31000
LogP:4.91280

Purity/Quality:

Safty Information:

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Technology Process of 3,5-BIS[(3-CHLOROPHENYL)METHYLENE]-1-METHYLTETRAHYDRO-4(1H)-PYRIDINONE

There total 1 articles about 3,5-BIS[(3-CHLOROPHENYL)METHYLENE]-1-METHYLTETRAHYDRO-4(1H)-PYRIDINONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 54237-29-5
3,5-bis-(3-chloro-benzylidene)-1-methyl-piperidin-4-one

Guidance literature:: N-Methyl-4-piperidinon, 3-Chlor-benzaldehyd;
DOI:10.1021/jm00188a018

Reference yield:

: 54237-29-5
3,5-bis-(3-chloro-benzylidene)-1-methyl-piperidin-4-one

: 109-77-3
malononitrile

: 1289514-54-0
(4R,8E)-2-amino-4-(3-chlorophenyl)-8-(3-chlorophenylmethylene)-5,6,7,8-tetrahydro-6-methyl-4H-pyrano[3,2-c]pyridine-3-carbonitrile

: 1446347-77-8
(4S,8E)-2-amino-4-(3-chlorophenyl)-8-(3-chlorophenylmethylene)-5,6,7,8-tetrahydro-6-methyl-4H-pyrano[3,2-c]pyridine-3-carbonitrile

Guidance literature:: With quinine; In toluene; at 20 ℃; for 36h; Overall yield = 99 %; enantioselective reaction;
DOI:10.3998/ark.5550190.0014.301