3-Furanpropanoic acid, 2-methyl-

Base Information

Chemical Name:3-Furanpropanoic acid, 2-methyl-
CAS No.:5554-98-3
Molecular Formula:C₈H₁₀O₃
Molecular Weight:154.166
Hs Code.:

Synonyms:

Suppliers and Price of 3-Furanpropanoic acid, 2-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
2-methyl-3-Furanpropanoicacid 97.00%
25G
$ 11900.00

AccelPharmtech
2-methyl-3-Furanpropanoicacid 97.00%
5G
$ 6320.00

AccelPharmtech
2-methyl-3-Furanpropanoicacid 97.00%
1G
$ 3660.00

Total 1 raw suppliers

Chemical Property of 3-Furanpropanoic acid, 2-methyl-

Chemical Property:

PSA：50.44000
LogP:1.60520

Purity/Quality:

95% ^*data from raw suppliers

2-methyl-3-Furanpropanoicacid 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-Furanpropanoic acid, 2-methyl-

There total 8 articles about 3-Furanpropanoic acid, 2-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 113541-58-5
ethyl 3-(2'-methyl-3'-furyl)propionate

: 5554-98-3
3-(2'-methyl-3'-furyl)propionic acid

Guidance literature:: With potassium hydroxide; at 90 ℃; for 3h;
DOI:10.1002/hlca.19870700524

Reference yield:

: 6947-94-0
2-methyl-3-furancarboxylic acid

: 5554-98-3
3-(2'-methyl-3'-furyl)propionic acid

Guidance literature:: Multi-step reaction with 7 steps

1: 92 percent / SOCl₂, pyridine / diethyl ether / 3 h / 0 - 30 °C

2: 1.) BuLi / 1.) hexane, -10 deg C; 2.) THF, -50 to 0 deg C, 20 min

3: 90 percent / NaBH₄ / ethanol / 0.33 h / 5 °C

4: 75 percent / pyridine / 18 h / Ambient temperature

5: 95 percent / K₂CO₃, alumina / 0.5 h / 180 °C

6: 82 percent / H₂ / Pd/C (5percent) / methanol / 1 h / 3040 Torr / Ambient temperature

7: 84 percent / KOH (20percent) / 3 h / 90 °C

With pyridine; aluminum oxide; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; thionyl chloride; hydrogen; potassium carbonate; palladium on activated charcoal; In pyridine; methanol; diethyl ether; ethanol;
DOI:10.1002/hlca.19870700524

Reference yield:

: 5555-00-0
2-methylfuran-3-carbonyl chloride

: 5554-98-3
3-(2'-methyl-3'-furyl)propionic acid

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) BuLi / 1.) hexane, -10 deg C; 2.) THF, -50 to 0 deg C, 20 min

2: 90 percent / NaBH₄ / ethanol / 0.33 h / 5 °C

3: 75 percent / pyridine / 18 h / Ambient temperature

4: 95 percent / K₂CO₃, alumina / 0.5 h / 180 °C

5: 82 percent / H₂ / Pd/C (5percent) / methanol / 1 h / 3040 Torr / Ambient temperature

6: 84 percent / KOH (20percent) / 3 h / 90 °C

With aluminum oxide; potassium hydroxide; sodium tetrahydroborate; n-butyllithium; hydrogen; potassium carbonate; palladium on activated charcoal; In pyridine; methanol; ethanol;
DOI:10.1002/hlca.19870700524