8-Isoquinolinamine,5-chloro-(9CI)

Base Information

• Chemical Name: 8-Isoquinolinamine,5-chloro-(9CI)
• CAS No.: 55766-82-0
• Molecular Formula: C9H7ClN2
• Molecular Weight: 178.61800
• Hs Code.: 2933499090
• Mol file: 55766-82-0.mol

Synonyms:5-chloro-isoquinolin-8-ylamine;8-Isoquinolinamine,5-chloro;8-Amino-5-chlor-isochinolin;8-amino-5-chloroisoquinoline;

Chemical Property of 8-Isoquinolinamine,5-chloro-(9CI)

Chemical Property:

• PSA: 38.91000
• LogP: 3.05160
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

5-chloroisoquinolin-8-amine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 8-Isoquinolinamine,5-chloro-(9CI)

There total 5 articles about 8-Isoquinolinamine,5-chloro-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-chloro-8-nitroisoquinoline (58142-95-3) → 5-chloro-8-isoquinolylamine (55766-82-0)

Guidance literature:

With methanol; palladium on activated charcoal; sodium acetate; Hydrogenation;

Reference yield:

5-chloro-isoquinoline (5430-45-5) → 5-chloro-8-isoquinolylamine (55766-82-0)

Guidance literature:

Multi-step reaction with 2 steps

1: concentrated sulfuric acid; potassium nitrate

2: SnCl₂; aqueous HCl

With hydrogenchloride; sulfuric acid; potassium nitrate; tin(ll) chloride;

Reference yield:

(3-chloro-benzylidenamino)-acetaldehyde diethylacetal → 5-chloro-8-isoquinolylamine (55766-82-0)

Guidance literature:

Multi-step reaction with 3 steps

1: concentrated sulfuric acid / Erhitzen des Rktgem_. mit Phosphor(V)-oxid auf 160grad

2: concentrated sulfuric acid; potassium nitrate

3: SnCl₂; aqueous HCl

With hydrogenchloride; sulfuric acid; potassium nitrate; tin(ll) chloride;

upstream raw materials:

5-chloro-8-nitroisoquinoline

5-chloro-isoquinoline

m-Chlorobenzaldehyde

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