3,5-Pyridinedicarboxylic acid, 2-[(1E)-2-chloro-2-(trimethylsilyl)ethenyl]-1,4-dihydro-6-methyl-4-(3-nitro phenyl)-, bis(1-methylethyl) ester

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 2-[(1E)-2-chloro-2-(trimethylsilyl)ethenyl]-1,4-dihydro-6-methyl-4-(3-nitro phenyl)-, bis(1-methylethyl) ester
CAS No.:557762-65-9
Molecular Formula:C₂₅H₃₃ClN₂O₆Si
Molecular Weight:521.085
Hs Code.:

3,5-Pyridinedicarboxylic acid,
2-[(1E)-2-chloro-2-(trimethylsilyl)ethenyl]-1,4-dihydro-6-methyl-4-(3-nitro
phenyl)-, bis(1-methylethyl) ester

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 2-[(1E)-2-chloro-2-(trimethylsilyl)ethenyl]-1,4-dihydro-6-methyl-4-(3-nitro phenyl)-, bis(1-methylethyl) ester

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Technology Process of 3,5-Pyridinedicarboxylic acid, 2-[(1E)-2-chloro-2-(trimethylsilyl)ethenyl]-1,4-dihydro-6-methyl-4-(3-nitro phenyl)-, bis(1-methylethyl) ester

There total 3 articles about 3,5-Pyridinedicarboxylic acid, 2-[(1E)-2-chloro-2-(trimethylsilyl)ethenyl]-1,4-dihydro-6-methyl-4-(3-nitro phenyl)-, bis(1-methylethyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 42201-71-8
methyl (trimethylsilyl)propiolate

: 557762-65-9
2-((E)-2-Chloro-2-trimethylsilanyl-vinyl)-6-methyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / LDA / tetrahydrofuran / -75 °C

2: 100 percent / piperidinium acetate / toluene / Heating

3: HCl / propan-2-ol / Heating

With hydrogenchloride; piperdinium acetate; lithium diisopropyl amide; In tetrahydrofuran; isopropyl alcohol; toluene; 2: Knoevenagel condensation;

Reference yield:

: 557762-56-8
iso-propyl 3-oxo-5-(trimethylsilanyl)pent-4-ynoate

: 557762-65-9
2-((E)-2-Chloro-2-trimethylsilanyl-vinyl)-6-methyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3,5-dicarboxylic acid diisopropyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / piperidinium acetate / toluene / Heating

2: HCl / propan-2-ol / Heating

With hydrogenchloride; piperdinium acetate; In isopropyl alcohol; toluene; 1: Knoevenagel condensation;