Piperidine, 4-[(4-bromophenyl)phenylmethylene]-

Base Information

Chemical Name:Piperidine, 4-[(4-bromophenyl)phenylmethylene]-
CAS No.:557795-45-6
Molecular Formula:C₁₈H₁₈BrN
Molecular Weight:328.252
Hs Code.:
DSSTox Substance ID:DTXSID70452794

Synonyms:Piperidine, 4-[(4-bromophenyl)phenylmethylene]-;557795-45-6;DTXSID70452794

Suppliers and Price of Piperidine, 4-[(4-bromophenyl)phenylmethylene]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Piperidine, 4-[(4-bromophenyl)phenylmethylene]-

Chemical Property:

XLogP3:4.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:327.06226
Heavy Atom Count:20
Complexity:327

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CNCCC1=C(C2=CC=CC=C2)C3=CC=C(C=C3)Br

Technology Process of Piperidine, 4-[(4-bromophenyl)phenylmethylene]-

There total 3 articles about Piperidine, 4-[(4-bromophenyl)phenylmethylene]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-[(4-bromo-phenyl)-hydroxy-phenyl-methyl]-piperidine-1-carboxylic acid tert-butyl ester

: 557795-45-6
4-bromo-[phenyl-(piperidin-4-ylidene)methyl]-benzene

Guidance literature:: With toluene-4-sulfonic acid; In benzene; for 2h; Heating;
DOI:10.1002/jlcr.651

Reference yield:

: 18620-02-5
(4-bromophenyl)magnesium bromide

: 557795-45-6
4-bromo-[phenyl-(piperidin-4-ylidene)methyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / Heating

2: 6.10 g / p-TsOH / benzene / 2 h / Heating

With toluene-4-sulfonic acid; In tetrahydrofuran; benzene; 1: Grignard reaction;
DOI:10.1002/jlcr.651

Reference yield:

: 193217-39-9
1-(t-butoxycarbonyl)-4-(benzoyl)piperidine

: 557795-45-6
4-bromo-[phenyl-(piperidin-4-ylidene)methyl]-benzene

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 2 h / Heating

2: 6.10 g / p-TsOH / benzene / 2 h / Heating

With toluene-4-sulfonic acid; In tetrahydrofuran; benzene; 1: Grignard reaction;
DOI:10.1002/jlcr.651