1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide

Base Information

Chemical Name:1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide
CAS No.:55781-96-9
Molecular Formula:C22H19OP
Molecular Weight:330.366
Hs Code.:
DSSTox Substance ID:DTXSID20464564
Nikkaji Number:J1.353.970G

Synonyms:1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide;55781-96-9;DTXSID20464564;1,3,4-triphenyl-3-phospholene oxide

Suppliers and Price of 1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide

Chemical Property:

XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:3
Exact Mass:330.117352223
Heavy Atom Count:24
Complexity:468

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C(=C(CP1(=O)C2=CC=CC=C2)C3=CC=CC=C3)C4=CC=CC=C4

Technology Process of 1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide

There total 7 articles about 1H-Phosphole, 2,5-dihydro-1,3,4-triphenyl-, 1-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 2548-47-2
2,3-diphenyl-1,3-butadiene

: 1073-47-8
phenyldibromophosphine

: 55781-96-9
1,3,4-Triphenyl-2,5-dihydrophosphole 1-oxide

Guidance literature:: With copper octadecanoate; In Petroleum ether; at 50 ℃; for 120h;
DOI:10.1021/ja00371a018

Reference yield:

: 2548-47-2
2,3-diphenyl-1,3-butadiene

: 55781-96-9
1,3,4-Triphenyl-2,5-dihydrophosphole 1-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: copper(II) stearate / petroleum ether / 384 h / 60 °C

2: 29.3 g / aq. NaHCO₃

With copper(II) stearate; sodium hydrogencarbonate; In Petroleum ether; 1: Cyclization / 2: Hydrolysis;
DOI:10.1039/b000692k