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Disilanamine, N,N-diethyl-2,2-dimethyl-1,1-diphenyl-2-(2-propenyl)-

Base Information
  • Chemical Name:Disilanamine, N,N-diethyl-2,2-dimethyl-1,1-diphenyl-2-(2-propenyl)-
  • CAS No.:558472-98-3
  • Molecular Formula:C21H31NSi2
  • Molecular Weight:353.655
  • Hs Code.:
Disilanamine, N,N-diethyl-2,2-dimethyl-1,1-diphenyl-2-(2-propenyl)-

Synonyms:

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Chemical Property of Disilanamine, N,N-diethyl-2,2-dimethyl-1,1-diphenyl-2-(2-propenyl)-
Chemical Property:
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Technology Process of Disilanamine, N,N-diethyl-2,2-dimethyl-1,1-diphenyl-2-(2-propenyl)-

There total 1 articles about Disilanamine, N,N-diethyl-2,2-dimethyl-1,1-diphenyl-2-(2-propenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
chloro(N,N-diethylamino)diphenylsilane; With lithium; In tetrahydrofuran; at 0 ℃; for 4h;
allyldimethylsilyl triflate; In tetrahydrofuran; diethyl ether; at 20 ℃; for 0.333333h;
Guidance literature:
In diethyl ether; at 0 ℃;
Guidance literature:
Multi-step reaction with 2 steps
1.1: diethyl ether / 0.5 h / 0 °C
2.1: Li / tetrahydrofuran / 4 h / 0 °C
2.2: tetrahydrofuran; diethyl ether / 2 h / 20 °C
With lithium; In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0022-328X(03)00158-X
upstream raw materials:

chloro(N,N-diethylamino)diphenylsilane

allyldimethylsilyl triflate

Downstream raw materials:

C18H21F3O3SSi2

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