sodium butyl trithiocarbonate

Base Information

• Chemical Name: sodium butyl trithiocarbonate
• CAS No.: 64773-45-1
• Molecular Formula: C5H10 S3 . Na
• Molecular Weight: 188.314
• Hs Code.: 2930909090
• Mol file: 64773-45-1.mol

Synonyms:Carbonicacid, trithio-, butyl ester, Na salt (6CI); Carbonotrithioic acid, monobutylester, sodium salt (9CI); Butyl sodium trithiocarbonate; n-Butyltrithiocarbonate sodium salt

Chemical Property of sodium butyl trithiocarbonate

Chemical Property:

• Vapor Pressure: 0.175mmHg at 25°C
• Boiling Point: 219.6°C at 760 mmHg
• Flash Point: 86.6°C
• PSA: 57.39000
• LogP: 2.35150

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium butyl trithiocarbonate

There total 1 articles about sodium butyl trithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

carbon disulfide (75-15-0,12122-00-8) + n-butanethiol (109-79-5) → butyl-trithiocarbonate de sodium (64773-45-1)

Guidance literature:

With sodium hydroxide;

DOI:10.1021/jo01308a020

Reference yield: 94.0%

1-chloro-2,4-dinitro-6-trifluoromethylbenzene (392-95-0) + butyl-trithiocarbonate de sodium (64773-45-1) → n-Butyl 2,4-dinitro-6-(trifluoromethyl)phenyl Trithiocarbonate (74512-02-0)

Guidance literature:

In acetone;

DOI:10.1021/jo01308a020

Reference yield: 90.0%

butyl-trithiocarbonate de sodium (64773-45-1) + cinnamyl chloride (2687-12-9) → S-cinnamyl butyl trithiocarbonate (123792-27-8)

Guidance literature:

In N,N-dimethyl-formamide;

DOI:10.1134/S1070427208090085

upstream raw materials:

carbon disulfide

n-butanethiol

Downstream raw materials:

n-Butyl 2,4-dinitro-6-(trifluoromethyl)phenyl Trithiocarbonate

S-cinnamyl butyl trithiocarbonate

Refernces

• 1、 Rasheed, Khalid,Warkentin, James D.. "Cyclization of Dinitrophenyl tert-Butyl Trithiocarbonates. A Novel Synthesis of Nitro-1,3-benzodithiole-2-thiones". . p. 4041 - 4044. Retrieved 2007/10/02.