Technology Process of Cyclobutanecarboxaldehyde,
1-(2,2-dimethoxyethyl)-2-[1-methyl-2-(phenylthio)ethyl]-
There total 8 articles about Cyclobutanecarboxaldehyde,
1-(2,2-dimethoxyethyl)-2-[1-methyl-2-(phenylthio)ethyl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sulfur trioxide pyridine complex; triethylamine;
In
dimethyl sulfoxide;
DOI:10.1021/ja00451a040
- Guidance literature:
-
Multi-step reaction with 7 steps
1: (i) nBuLi, THF, (ii) /BRN= 1817781/, (iii) TsOH, benzene
2: (i) nBuLi, (ii) /BRN= 2503992/
3: TsOH / benzene
4: pyridinium bromide perbromide / acetic acid
5: AgNO3
6: LiAlH4 / tetrahydrofuran
7: Et3N, Py*SO3 / dimethylsulfoxide
With
lithium aluminium tetrahydride; pyridinium hydrobromide perbromide; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; silver nitrate; triethylamine;
In
tetrahydrofuran; acetic acid; dimethyl sulfoxide; benzene;
DOI:10.1021/ja00451a040
- Guidance literature:
-
Multi-step reaction with 6 steps
1: (i) nBuLi, (ii) /BRN= 2503992/
2: TsOH / benzene
3: pyridinium bromide perbromide / acetic acid
4: AgNO3
5: LiAlH4 / tetrahydrofuran
6: Et3N, Py*SO3 / dimethylsulfoxide
With
lithium aluminium tetrahydride; pyridinium hydrobromide perbromide; sulfur trioxide pyridine complex; toluene-4-sulfonic acid; silver nitrate; triethylamine;
In
tetrahydrofuran; acetic acid; dimethyl sulfoxide; benzene;
DOI:10.1021/ja00451a040