Cyclobutanepropanoic acid, α-amino-, ethyl ester, hydrochloride

Base Information

• Chemical Name: Cyclobutanepropanoic acid, α-amino-, ethyl ester, hydrochloride
• CAS No.: 565456-74-8
• Molecular Formula: C9H17NO2.ClH
• Molecular Weight: 207.69800
• Mol file: 565456-74-8.mol

Synonyms:

Chemical Property of Cyclobutanepropanoic acid, α-amino-, ethyl ester, hydrochloride

Chemical Property:

• PSA: 52.32000
• LogP: 2.56930

Purity/Quality:

97% ^*data from raw suppliers

Ethyl2-Amino-3-cyclobutylpropanoateHydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Cyclobutanepropanoic acid, α-amino-, ethyl ester, hydrochloride

There total 4 articles about Cyclobutanepropanoic acid, α-amino-, ethyl ester, hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Bromomethyl)cyclobutane (17247-58-4) + ethyl N-diphenylmethylene glycine (69555-14-2) → C9H17NO2*ClH (565456-74-8)

Guidance literature:

With potassium tert-butylate; In tetrahydrofuran; at -78 - 20 ℃; for 49h;

Reference yield:

2-(benzhydrylidene-amino)-3-cyclobutyl-propionic acid ethyl ester (1025799-39-6) → C9H17NO2*ClH (565456-74-8)

Guidance literature:

With hydrogenchloride; water; In diethyl ether; at 20 ℃; for 5h;

Reference yield:

ethyl 2-amino-3-cyclobutylpropanoate (394735-17-2) → C9H17NO2*ClH (565456-74-8)

Guidance literature:

ethyl 2-amino-3-cyclobutylpropanoate; With hydrogenchloride; In diethyl ether; water; at 20 ℃; for 5h;

With sodium hydroxide; In diethyl ether; water; at 20 ℃; for 48h; pH=~ 12 - 14;

upstream raw materials:

(Bromomethyl)cyclobutane

ethyl N-diphenylmethylene glycine

ethyl 2-amino-3-cyclobutylpropanoate

2-(benzhydrylidene-amino)-3-cyclobutyl-propionic acid ethyl ester

Downstream raw materials:

ethyl 2-(tert-butoxycarbonylamino)-3-cyclobutylpropanoate

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