Carbamic acid, (trans-4-aminocyclohexyl)-, butyl ester

Base Information

Chemical Name:Carbamic acid, (trans-4-aminocyclohexyl)-, butyl ester
CAS No.:566172-78-9
Molecular Formula:C11H22N2O2
Molecular Weight:214.308
Hs Code.:

Synonyms:

Suppliers and Price of Carbamic acid, (trans-4-aminocyclohexyl)-, butyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Carbamic acid, (trans-4-aminocyclohexyl)-, butyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Carbamic acid, (trans-4-aminocyclohexyl)-, butyl ester

There total 1 articles about Carbamic acid, (trans-4-aminocyclohexyl)-, butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 52.0%

: 2615-25-0
trans-1,4-cyclohexyldiamine

: 592-34-7
carbonochloridic acid, butyl ester

: 566172-78-9
n-butyl trans-(4-aminocyclohexyl)-carbamate

: 901528-99-2
C₁₆H₃₀N₂O₄

Guidance literature:: trans-1,4-cyclohexyldiamine; carbonochloridic acid, butyl ester; In dichloromethane; at 0 - 10 ℃; for 1 - 1.16667h;

With sodium carbonate; In dichloromethane; water; at 20 ℃; for 0.0833333h;

Reference yield: 91.0%

: 566172-78-9
n-butyl trans-(4-aminocyclohexyl)-carbamate

: 15803-59-5,1932261-28-3,38362-02-6
(1r,4r)-N¹-methylcyclohexane-1,4-diamine

Guidance literature:: n-butyl trans-(4-aminocyclohexyl)-carbamate; With lithium aluminium tetrahydride; In tetrahydrofuran; at 0 ℃; for 18.5h; Heating / reflux;

With sodium hydroxide; water; In tetrahydrofuran; at 0 - 20 ℃; for 2.16h;

Reference yield:

: 566172-78-9
n-butyl trans-(4-aminocyclohexyl)-carbamate

: 1025061-58-8
C₃₅H₄₂ClN₅O₄S

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 18.5 h / 0 °C / Heating / reflux

1.2: 2.16 h / 0 - 20 °C

2.1: benzaldehyde / toluene / 6 h / Heating / reflux

2.2: 3.25 h / 20 °C

3.1: acetic acid / tetrahydrofuran; methanol; toluene / 4 h / 20 °C

3.2: 1 h

4.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 16 h / 20 °C

5.1: caesium carbonate / tetrakis(triphenylphosphine) palladium⁽⁰⁾ / ethanol; toluene / 16.16 h / 110 °C

With lithium aluminium tetrahydride; caesium carbonate; benzaldehyde; acetic acid; N-ethyl-N,N-diisopropylamine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; methanol; ethanol; dichloromethane; toluene; 5.1: Suzuki Coupling;