Technology Process of Septorin
There total 11 articles about Septorin which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrogenchloride;
In
methanol;
for 8h;
Ambient temperature;
DOI:10.3987/COM-91-5682
- Guidance literature:
-
Multi-step reaction with 7 steps
1: 43 percent / benzeneselenic anhydride (BSA) / chlorobenzene / 6 h
2: 1.) Mg, I2 / 1.) Et2O, THF, reflux, 30 min, 2.) Et2O, THF, RT, 6 h
3: 98 percent / permaleic acid / CHCl3
4: 99 percent / Collins reagent / CH2Cl2 / 3 h / Ambient temperature
5: 97 percent / 6 h / Heating
6: 99 percent / 10percent K2CO3, MeOH / 0.5 h / Heating
7: 95 percent / conc. HCl / methanol / 8 h / Ambient temperature
With
hydrogenchloride; methanol; monopermaleic acid; Collins oxidation agent; benzeneseleninic anhydride; iodine; potassium carbonate; magnesium;
In
methanol; dichloromethane; chloroform; chlorobenzene;
DOI:10.3987/COM-91-5682
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 1.) Mg, I2 / 1.) Et2O, THF, reflux, 30 min, 2.) Et2O, THF, RT, 6 h
2: 98 percent / permaleic acid / CHCl3
3: 99 percent / Collins reagent / CH2Cl2 / 3 h / Ambient temperature
4: 97 percent / 6 h / Heating
5: 99 percent / 10percent K2CO3, MeOH / 0.5 h / Heating
6: 95 percent / conc. HCl / methanol / 8 h / Ambient temperature
With
hydrogenchloride; methanol; monopermaleic acid; Collins oxidation agent; iodine; potassium carbonate; magnesium;
In
methanol; dichloromethane; chloroform;
DOI:10.3987/COM-91-5682
