Technology Process of Carbonocyanidic acid, (4-methoxyphenyl)methyl ester
There total 2 articles about Carbonocyanidic acid, (4-methoxyphenyl)methyl ester which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
diethylamino-sulfur trifluoride;
In
dichloromethane;
at 0 ℃;
for 0.5h;
Inert atmosphere;
DOI:10.1016/j.tetlet.2021.153116
- Guidance literature:
-
Multi-step reaction with 2 steps
1: n-Butyl nitrite; hydrogenchloride / tetrahydrofuran; 1,4-dioxane / 1 h / 20 °C / Inert atmosphere
2: diethylamino-sulfur trifluoride / dichloromethane / 0.5 h / 0 °C / Inert atmosphere
With
hydrogenchloride; n-Butyl nitrite; diethylamino-sulfur trifluoride;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1016/j.tetlet.2021.153116
- Guidance literature:
-
With
N,N,N,N,N,N-hexamethylphosphoric triamide; lithium diisopropyl amide;
Yield given. Multistep reaction;
1.) THF, 0 deg C; 2.) THF, -78 deg C to r.t.;
DOI:10.1021/ja00243a062
