1,2,4,5-tetrachloro-3-fluorobenzene

Base Information

• Chemical Name: 1,2,4,5-tetrachloro-3-fluorobenzene
• CAS No.: 319-97-1
• Molecular Formula: C6H Cl4 F
• Molecular Weight: 233.8825
• Mol file: 319-97-1.mol

Synonyms:1,2,4,5-Tetrachloro-3-fluorobenzene;1-Fluoro-2,3,5,6-tetrachlorobenzene; 2,3,5,6-Tetrachlorofluorobenzene

Chemical Property of 1,2,4,5-tetrachloro-3-fluorobenzene

Chemical Property:

• Vapor Pressure: 0.0485mmHg at 25°C
• Boiling Point: 244°Cat760mmHg
• Flash Point: 109.4°C
• PSA: 0.00000
• Density: 1.653g/cm³
• LogP: 4.43930

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,2,4,5-tetrachloro-3-fluorobenzene

There total 4 articles about 1,2,4,5-tetrachloro-3-fluorobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

2,3,5,6-Tetrachloronitrobenzene (117-18-0) → 2,3,5,6-tetrachlorofluorobenzene (319-97-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; for 1.5h; Ambient temperature;

DOI:10.1016/S0040-4039(00)98970-6

Reference yield:

2,3,5,6-tetrachlorobenzene-1-sulfonyl chloride (26120-84-3) → 2,3,5,6-tetrachlorofluorobenzene (319-97-1)

Guidance literature:

With potassium fluoride; at 230 ℃;

Reference yield:

3,5,6-Trichlor-2-fluor-benzolsulfofluorid (13656-47-8) → 2,3,5,6-tetrachlorofluorobenzene (319-97-1)

Guidance literature:

Irradiation;

upstream raw materials:

2,3,5,6-Tetrachloronitrobenzene

3,5,6-Trichlor-2-fluor-benzolsulfofluorid

2,3,5,6-tetrachlorobenzene-1-sulfonyl chloride

Downstream raw materials:

1-Fluor-4-nitrotetrachlorbenzol

2,3,5,6-Tetrachlorobenzenethiol

2,3,5,6-Tetrachlor-N-methyl-anilin

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