Benzenamine, 4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen yl]-

Base Information

Chemical Name:Benzenamine, 4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen yl]-
CAS No.:572900-60-8
Molecular Formula:C48H30N4O6S3
Molecular Weight:854.987
Hs Code.:

Synonyms:

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Chemical Property of Benzenamine, 4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen yl]-

Chemical Property:

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Technology Process of Benzenamine, 4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen yl]-

There total 1 articles about Benzenamine, 4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen yl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 586-78-7
para-nitrophenyl bromide

: 142807-63-4
tris(4-(thiophen-2-yl)phenyl)amine

: 572900-60-8
tris-{4-[5-(4-nitro-phenyl)-thiophen-2-yl]-phenyl}-amine

Guidance literature:: tris(4-(thiophen-2-yl)phenyl)amine; With n-butyllithium; In tetrahydrofuran; hexane; at -78 - 20 ℃;

With zinc(II) chloride; In tetrahydrofuran; hexane; at 20 ℃;

para-nitrophenyl bromide; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; hexane; at 20 ℃; for 24h;
DOI:10.1021/ja050765c

Reference yield:

: 572900-60-8
tris-{4-[5-(4-nitro-phenyl)-thiophen-2-yl]-phenyl}-amine

: 572900-58-4
C₄₈H₃₆N₄S₃

Guidance literature:: With NaBH₂S₃; In tetrahydrofuran; for 24h; Heating;
DOI:10.1021/ja050765c

Reference yield:

: 572900-60-8
tris-{4-[5-(4-nitro-phenyl)-thiophen-2-yl]-phenyl}-amine

: C₈₇H₆₀N₄S₃

Guidance literature:: Multi-step reaction with 2 steps

1: 0.15 g / NaBH₂S₃ / tetrahydrofuran / 24 h / Heating

2: 94 percent / DABCO; TiCl₄ / chlorobenzene / 125 °C

With 1,4-diaza-bicyclo[2.2.2]octane; NaBH₂S₃; titanium tetrachloride; In tetrahydrofuran; chlorobenzene;
DOI:10.1021/ja050765c