Technology Process of Benzenamine,
4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen
yl]-
There total 1 articles about Benzenamine,
4-[5-(4-nitrophenyl)-2-thienyl]-N,N-bis[4-[5-(4-nitrophenyl)-2-thienyl]phen
yl]- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
tris(4-(thiophen-2-yl)phenyl)amine;
With
n-butyllithium;
In
tetrahydrofuran; hexane;
at -78 - 20 ℃;
With
zinc(II) chloride;
In
tetrahydrofuran; hexane;
at 20 ℃;
para-nitrophenyl bromide;
With
tetrakis(triphenylphosphine) palladium(0);
In
tetrahydrofuran; hexane;
at 20 ℃;
for 24h;
DOI:10.1021/ja050765c
- Guidance literature:
-
With
NaBH2S3;
In
tetrahydrofuran;
for 24h;
Heating;
DOI:10.1021/ja050765c
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 0.15 g / NaBH2S3 / tetrahydrofuran / 24 h / Heating
2: 94 percent / DABCO; TiCl4 / chlorobenzene / 125 °C
With
1,4-diaza-bicyclo[2.2.2]octane; NaBH2S3; titanium tetrachloride;
In
tetrahydrofuran; chlorobenzene;
DOI:10.1021/ja050765c
