1-Phenylcyclohepta-1,3-diene

Base Information

Chemical Name:1-Phenylcyclohepta-1,3-diene
CAS No.:57293-43-3
Molecular Formula:C13H14
Molecular Weight:170.254
Hs Code.:
DSSTox Substance ID:DTXSID90498477
Nikkaji Number:J1.151.665C

Synonyms:1-Phenylcyclohepta-1,3-diene;phenylcycloheptadiene;57293-43-3;DTXSID90498477

Suppliers and Price of 1-Phenylcyclohepta-1,3-diene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Phenylcyclohepta-1,3-diene

Chemical Property:

XLogP3:3.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:1
Exact Mass:170.109550447
Heavy Atom Count:13
Complexity:204

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC=CC=C(C1)C2=CC=CC=C2

Technology Process of 1-Phenylcyclohepta-1,3-diene

There total 11 articles about 1-Phenylcyclohepta-1,3-diene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 68099-19-4
(RS)-1-phenyl-cyclohept-2-en-1-ol

: 57293-43-3
1-phenyl-1,3-cycloheptadiene

Guidance literature:: With 2,4-dinitrobenzenesulfenyl chloride; triethylamine; In dichloromethane; for 2.5h; Ambient temperature;
DOI:10.1021/ja00389a028

Reference yield: 38.0%

: 68099-19-4
(RS)-1-phenyl-cyclohept-2-en-1-ol

: 57293-43-3
1-phenyl-1,3-cycloheptadiene

: 147068-27-7
3-phenyl-2-cyclohepten-1-one

Guidance literature:: With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In dimethyl sulfoxide; at 55 ℃; for 1h;
DOI:10.1021/ol048210u

Reference yield:

: 1121-66-0
2-Cyclohepten-1-one

: 57293-43-3
1-phenyl-1,3-cycloheptadiene

Guidance literature:: Multi-step reaction with 2 steps

1: cyclohexane; diethyl ether; tetrahydrofuran / 1 h / -78 °C

2: 53 percent / 1-hydroxy-1,2-benziodoxal-3(1H)-one-1-oxide / dimethylsulfoxide / 1 h / 55 °C

With 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; diethyl ether; cyclohexane; dimethyl sulfoxide;
DOI:10.1021/ol048210u