Hexahydro-1H-cyclopenta[c]furan-1-one

Base Information

Chemical Name:Hexahydro-1H-cyclopenta[c]furan-1-one
CAS No.:5733-03-9
Molecular Formula:C7H10O2
Molecular Weight:126.155
Hs Code.:2932209090
DSSTox Substance ID:DTXSID30505659
Nikkaji Number:J464.750E

Synonyms:Hexahydro-1H-cyclopenta[c]furan-1-one;5733-03-9;hexahydro-cyclopenta[c]furan-1-one;rac-(3aR,6aS)-hexahydro-1H-cyclopenta[c]furan-1-one, cis;113428-55-0;SCHEMBL56213;DTXSID30505659;MFCD29033818;AS-0653;SB37735;E85832;EN300-219099

Suppliers and Price of Hexahydro-1H-cyclopenta[c]furan-1-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of Hexahydro-1H-cyclopenta[c]furan-1-one

Chemical Property:

PSA：26.30000
LogP:0.95950
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:126.068079557
Heavy Atom Count:9
Complexity:142

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CC2COC(=O)C2C1

Technology Process of Hexahydro-1H-cyclopenta[c]furan-1-one

There total 2 articles about Hexahydro-1H-cyclopenta[c]furan-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 41.6%

: 113335-69-6
2-Iodo-hept-6-enoic acid methyl ester

: 113428-55-0,5733-03-9,75658-84-3,82442-63-5,121960-86-9
hexahydro-cyclopenta[c]furan-1-one

: 113335-86-7,113335-87-8
3-Iodo-cyclohexanecarboxylic acid methyl ester

: 113335-78-7
cis-methyl 2-(iodomethyl)cyclopentanecarboxylate

: 113335-79-8
trans-methyl 2-(iodomethyl)cyclopentanecarboxylate

Guidance literature:: With 2,2'-azobis(isobutyronitrile); In benzene; for 1h; Heating;
DOI:10.1021/jo00274a034

Reference yield: 17.0%

: 113335-71-0
2-Iodo-hept-6-enoic acid tert-butyl ester

: 113428-55-0,5733-03-9,75658-84-3,82442-63-5,121960-86-9
hexahydro-cyclopenta[c]furan-1-one

: 113335-81-2
trans-tert-butyl 2-(iodomethyl)cyclopentanecarboxylate

: 113335-80-1
cis-tert-butyl 2-(iodomethyl)cyclopentanecarboxylate

: 113335-89-0
trans-tert-butyl 3-iodocyclohexanecarboxylate

Guidance literature:: With hexamethyldistannane; Di-tert-butylpyridine; In benzene; at 60 - 80 ℃; for 0.166667h; Further byproducts given; Irradiation;
DOI:10.1021/jo00274a034

Reference yield: 62.0%

: 104-92-7
1-bromo-4-methoxy-benzene

: 113428-55-0,5733-03-9,75658-84-3,82442-63-5,121960-86-9
hexahydro-cyclopenta[c]furan-1-one

: (3aR,6aS)-6a-(4-Methoxy-phenyl)-hexahydro-cyclopenta[c]furan-1-one

Guidance literature:: With tri-tert-butyl phosphine; lithium hexamethyldisilazane; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In toluene; at 140 ℃; for 0.166667h; microwave irradiation;
DOI:10.1016/j.tetlet.2005.08.030