3-Cyclohexene-1,1-dicarboxylic acid, 3-chloro-, diethyl ester

Base Information

• Chemical Name: 3-Cyclohexene-1,1-dicarboxylic acid, 3-chloro-, diethyl ester
• CAS No.: 575501-28-9
• Molecular Formula: C12H17ClO4
• Molecular Weight: 260.718
• DSSTox Substance ID: DTXSID50464471
• Nikkaji Number: J1.929.685G
• Mol file: 575501-28-9.mol

Synonyms:575501-28-9;3-Cyclohexene-1,1-dicarboxylic acid, 3-chloro-, diethyl ester;DTXSID50464471

Chemical Property of 3-Cyclohexene-1,1-dicarboxylic acid, 3-chloro-, diethyl ester

Chemical Property:

• XLogP3: 2.6
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 6
• Exact Mass: 260.0815367
• Heavy Atom Count: 17
• Complexity: 317

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCOC(=O)C1(CCC=C(C1)Cl)C(=O)OCC

Technology Process of 3-Cyclohexene-1,1-dicarboxylic acid, 3-chloro-, diethyl ester

There total 3 articles about 3-Cyclohexene-1,1-dicarboxylic acid, 3-chloro-, diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

2-but-3-enyl-2-(2-chloro-allyl)-malonic acid diethyl ester → 3-chloro-cyclohex-3-ene-1,1-dicarboxylic acid diethyl ester (575501-28-9)

Guidance literature:

tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In benzene; at 65 ℃; for 6h;

DOI:10.1021/ol034775z

Reference yield: 98.0%

2-(2-Chloro-allyl)-2-((Z)-pent-3-enyl)-malonic acid diethyl ester → 3-chloro-cyclohex-3-ene-1,1-dicarboxylic acid diethyl ester (575501-28-9)

Guidance literature:

tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In benzene; at 65 ℃; for 6h;

DOI:10.1021/ol034775z

Reference yield: 98.0%

2-(2-Chloro-allyl)-2-((E)-pent-3-enyl)-malonic acid diethyl ester → 3-chloro-cyclohex-3-ene-1,1-dicarboxylic acid diethyl ester (575501-28-9)

Guidance literature:

tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; In benzene; at 65 ℃; for 2h;

DOI:10.1055/s-2004-822327