N-(1-Thioxoethyl)-L-tryptophan methyl ester

Base Information

Chemical Name:N-(1-Thioxoethyl)-L-tryptophan methyl ester
CAS No.:54774-15-1
Molecular Formula:C14H16N2O2S
Molecular Weight:276.354
Hs Code.:
DSSTox Substance ID:DTXSID90203240
Wikidata:Q76150856

Synonyms:N-(1-Thioxoethyl)-L-tryptophan methyl ester;L-Tryptophan, N-(1-thioxoethyl)-, methyl ester;54774-15-1;DTXSID90203240;LS-158168

Suppliers and Price of N-(1-Thioxoethyl)-L-tryptophan methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(1-Thioxoethyl)-L-tryptophan methyl ester

Chemical Property:

Vapor Pressure:7.78E-09mmHg at 25°C
Boiling Point:465.3°Cat760mmHg
Flash Point:235.2°C
Density:1.265g/cm³
XLogP3:2
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:276.09324893
Heavy Atom Count:19
Complexity:348

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=S)NC(CC1=CNC2=CC=CC=C21)C(=O)OC
Isomeric SMILES:CC(=S)N[C@@H](CC1=CNC2=CC=CC=C21)C(=O)OC

Technology Process of N-(1-Thioxoethyl)-L-tryptophan methyl ester

There total 2 articles about N-(1-Thioxoethyl)-L-tryptophan methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 2824-57-9,16108-06-8,36060-94-3
N-acetyl-L-tryptophan methyl ester

: 54774-15-1
(S)-(+)-methylthiocarbonyl tryptophan methyl ester

Guidance literature:: With Lawessons reagent;
DOI:10.1248/cpb.33.3237

Reference yield:

: 2717-75-1
N-benzoyl-L-tryptophan methyl ester

: 54774-15-1
(S)-(+)-methylthiocarbonyl tryptophan methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / CH₃I / methanol / 24 h / Ambient temperature

2: 98 percent / Lawesson's reagent

With Lawessons reagent; methyl iodide; In methanol;
DOI:10.1248/cpb.33.3237

Reference yield:

: 10022-77-2,54774-15-1,81801-79-8,93712-57-3
3-(1H-Indol-3-yl)-2-thioacetylamino-propionic acid methyl ester

: 16108-10-4,34368-37-1,34368-38-2,50302-68-6,55449-00-8,75196-51-9,93598-06-2,123809-87-0,147976-41-8
(1S,3S)-1-Methyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) methyl iodide / 1.) acetone, 2.) reflux

2: 90 percent / NaBH₄

With sodium tetrahydroborate; methyl iodide;