(3-methylbutyl)(diphenyl)phosphane oxide

Base Information

Chemical Name:(3-methylbutyl)(diphenyl)phosphane oxide
CAS No.:46941-66-6
Molecular Formula:C17H21OP
Molecular Weight:272.327
Hs Code.:
Mol file:46941-66-6.mol

Synonyms:

Suppliers and Price of (3-methylbutyl)(diphenyl)phosphane oxide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (3-methylbutyl)(diphenyl)phosphane oxide

Chemical Property:

Vapor Pressure:3.51E-05mmHg at 25°C
Boiling Point:364.5°Cat760mmHg
Flash Point:174.2°C
Density:1.05g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (3-methylbutyl)(diphenyl)phosphane oxide

There total 13 articles about (3-methylbutyl)(diphenyl)phosphane oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 4145-83-9
(3-methylbuta-1,2-dien-1-yl)diphenylphosphine oxide

: 46941-66-6
(3-methylbutan-1-yl)(diphenyl)phosphine oxide

Guidance literature:: With palladium 10% on activated carbon; hydrogen; In methanol; at 25 ℃; for 24h; under 760.051 Torr;
DOI:10.1134/S1070428017070065

Reference yield: 95.0%

: 603-35-0
triphenylphosphine

: 107-82-4
i-pentyl bromide

: 46941-66-6
(3-methylbutan-1-yl)(diphenyl)phosphine oxide

Guidance literature:: triphenylphosphine; i-pentyl bromide; Reflux; Inert atmosphere;

With sodium hydroxide; In diethyl ether; water; for 2h; Inert atmosphere; Heating;
DOI:10.1002/adsc.201400861

Reference yield: 78.0%

: 714956-55-5
(3-methyl-3-butenyl)diphenylphosphine-borane complex

: 46941-66-6
(3-methylbutan-1-yl)(diphenyl)phosphine oxide

: 126338-44-1,136492-22-3
(4-diphenylphosphinoyl)-2-methyl-1-butanol

Guidance literature:: (3-methyl-3-butenyl)diphenylphosphine-borane complex; With methanesulfonic acid; In dichloromethane; at 20 ℃; for 0.166667h; Inert atmosphere;

With dihydrogen peroxide; sodium hydroxide; In methanol; dichloromethane; water; at 20 ℃; for 1h; Inert atmosphere;
DOI:10.1021/ol2031203