Benzoic acid, 4-nitro-, copper(2+) salt

Base Information

• Chemical Name: Benzoic acid, 4-nitro-, copper(2+) salt
• CAS No.: 5819-29-4
• Molecular Formula: 2C₇H₄NO₄*Cu
• Molecular Weight: 395.772
• Mol file: 5819-29-4.mol

Synonyms:

Chemical Property of Benzoic acid, 4-nitro-, copper(2+) salt

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 4-nitro-, copper(2+) salt

There total 2 articles about Benzoic acid, 4-nitro-, copper(2+) salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

copper dichloride + 4-nitro-benzoic acid (62-23-7) → copper(II) 4-nitrobenzoate (5819-29-4,35425-38-8,127223-70-5)

Guidance literature:

With NaOH; In water; acetone; neutralization of nitrobenzoic acid soln. (acetone) by aq. NaOH soln., addn. of small excess of acid, filtration, addn. of filtrate to aq. metal chloride soln., stirring (0.5 h); filtration, washing (water), drying (air, than vac. 140°C, 4 h);

DOI:10.1016/S0277-5387(00)80303-4

Reference yield:

copper(II) p-nitrobenzoate monohydrate (20161-00-6,38724-13-9) → copper(II) 4-nitrobenzoate (5819-29-4,35425-38-8,127223-70-5)

Guidance literature:

In not given; on heating at 105-160°C;;

Reference yield: 78.0%

Quinoline N-oxide (1613-37-2) + copper(II) 4-nitrobenzoate (5819-29-4,35425-38-8,127223-70-5) → [bis(4-nitrobenzoate)quinoline N-oxide-copper(II)]2 (91730-68-6)

Guidance literature:

In not given; mixing the carboxylate and the ligand in an org. solvent, procedure similar to the method described by N. Kumar et al., Proc. Indian Natn. Sci.Acad., 49A (1983) 404; elem. anal.;

upstream raw materials:

4-nitro-benzoic acid

copper(II) p-nitrobenzoate monohydrate

Downstream raw materials:

Cu(4-O₂NC₆H₄COO)2(1-methylpiperazine)2

Cu(4-O₂NC₆H₄COO)2(3-methylpiperidine)2

[bis(4-nitrobenzoate)quinoline N-oxide-copper(II)]2

[Cu(C₁₉H₁₈N₃O)(O₂CC₆H₄NO₂)]