2-[(Benzylimino)methyl]-4,6-dichlorophenol

Base Information

Chemical Name:2-[(Benzylimino)methyl]-4,6-dichlorophenol
CAS No.:58199-78-3
Molecular Formula:C₁₄H₁₁Cl₂NO
Molecular Weight:280.153
Hs Code.:
DSSTox Substance ID:DTXSID40425298
Nikkaji Number:J658.038F

Synonyms:2-[(benzylimino)methyl]-4,6-dichlorophenol;58199-78-3;Phenol, 2,4-dichloro-6-[[(phenylmethyl)imino]methyl]-;DTXSID40425298;3,5-dichlorosalicylidene-benzylamine;AKOS003410311

Suppliers and Price of 2-[(Benzylimino)methyl]-4,6-dichlorophenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2-[(Benzylimino)methyl]-4,6-dichlorophenol

Chemical Property:

XLogP3:4.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:279.0217694
Heavy Atom Count:18
Complexity:279

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)CN=CC2=C(C(=CC(=C2)Cl)Cl)O

Technology Process of 2-[(Benzylimino)methyl]-4,6-dichlorophenol

There total 2 articles about 2-[(Benzylimino)methyl]-4,6-dichlorophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 100-46-9
benzylamine

: 90-60-8
3,5-dichlorosalicyclaldehyde

: 58199-78-3
2,4-dichloro-6-((benzylimino)methyl)phenol

Guidance literature:: With magnesium sulfate; In toluene; for 4h; Inert atmosphere; Reflux;
DOI:10.1039/c8dt02140f

Reference yield:

: 58199-78-3
2,4-dichloro-6-((benzylimino)methyl)phenol

Guidance literature:: 3,5-Dichlor-salicylaldehyd, Benzylamin, Aethanol, Erwaermen;

Reference yield: 36.0%

: diacetatobis(3,5-dimethylpyridine)palladium(II)

: 58199-78-3
2,4-dichloro-6-((benzylimino)methyl)phenol

: 201213-26-5
Pd(OC₆H₂Cl₂CHNCH₂C₆H₅)(CH₃COO)(3,5-dimethylpyridine)

Guidance literature:: In benzene; stirring equimolar amts. (50°C, 2 h); evapn., recrystn. (C6H6/hexane); elem. anal.;
DOI:10.1016/S0022-328X(97)00377-X