AKOS 91763

Base Information

Chemical Name:AKOS 91763
CAS No.:61394-53-4
Molecular Formula:C9H8ClNOS
Molecular Weight:213.6839
Hs Code.:
Mol file:61394-53-4.mol

Synonyms:5-Chlor-3-methylthiooxindol;5-chloro-3-methylthio-oxindole;5-Chlor-3-methylthioxindol;5-chloro-3-methylsulfanyl-1,3-dihydro-indol-2-one;

Suppliers and Price of AKOS 91763

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

AccelPharmtech
5-chloro-1,3-dihydro-3-(methylthio)-2H-Indol-2-one 97.00%
25G
$ 4320.00

AccelPharmtech
5-chloro-1,3-dihydro-3-(methylthio)-2H-Indol-2-one 97.00%
5G
$ 2330.00

AccelPharmtech
5-chloro-1,3-dihydro-3-(methylthio)-2H-Indol-2-one 97.00%
1G
$ 2070.00

Total 4 raw suppliers

Chemical Property of AKOS 91763

Chemical Property:

Vapor Pressure:8.58E-06mmHg at 25°C
Boiling Point:374.1°C at 760 mmHg
Flash Point:180°C
PSA：54.40000
Density:1.41g/cm³
LogP:2.83420

Purity/Quality:

85.0-99.8% ^*data from raw suppliers

5-chloro-1,3-dihydro-3-(methylthio)-2H-Indol-2-one 97.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of AKOS 91763

There total 5 articles about AKOS 91763 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 2-(2-amino-5-chlorophenyl)-2-(methylthio)acetamide

: 61394-53-4
5-Chlor-3-methylthiooxindol

Guidance literature:: With hydrogenchloride; In water; at 20 ℃;
DOI:10.1016/j.tetlet.2014.08.044

Reference yield: 59.0%

: 16630-66-3
methyl 2-(methylthio)acetate

: 106-47-8
4-chloro-aniline

: 61394-53-4
5-Chlor-3-methylthiooxindol

Guidance literature:: methyl 2-(methylthio)acetate; 4-chloro-aniline; With sulfuryl dichloride; In acetic acid butyl ester; at -30 ℃; for 0.5h; Inert atmosphere;

With hydrogenchloride; In methanol; acetic acid butyl ester; water; for 16h; Inert atmosphere;

Reference yield:

: 106-47-8
4-chloro-aniline

: 61394-53-4
5-Chlor-3-methylthiooxindol

Guidance literature:: Multi-step reaction with 2 steps

1.1: N-chlorophthalimide / dichloromethane / 2 h / -20 - -15 °C

1.2: -8 °C

2.1: hydrogenchloride / water / 20 °C

With hydrogenchloride; N-chlorophthalimide; In dichloromethane; water;
DOI:10.1016/j.tetlet.2014.08.044