Germane, chlorotris(4-methylphenyl)-

Base Information

Chemical Name:Germane, chlorotris(4-methylphenyl)-
CAS No.:58436-48-9
Molecular Formula:C21H21ClGe
Molecular Weight:381.441
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Germane, chlorotris(4-methylphenyl)-

Chemical Property:

Purity/Quality:

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Pictogram(s):
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MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Germane, chlorotris(4-methylphenyl)-

There total 1 articles about Germane, chlorotris(4-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 106-43-4
para-chlorotoluene

: 10038-98-9
germaniumtetrachloride

: 58436-48-9
tri(p-tolyl)chlorogermane

Guidance literature:: With aq. HCl; Mg; I₂; In tetrahydrofuran; Schlenk, glove box technique, under N2; part of CH3C6H4Cl (117.9 mmol) soln. added to Mg (177 mmol), I2 added, heated, CH3C6H4Cl added, refluxed(2 h), cooled, soln. of GeCl4 (39.3 mmol) added, refluxed (90 min), coo led, poured over aq. HCl (0°C); THF layer sepd., aq. layer extracted with ether, THF layer and ethered layer combined, dried over MgSO4, filtered, volatiles removed, distilled in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2010.04.015

Reference yield: 76.0%

: 58436-48-9
tri(p-tolyl)chlorogermane

: 3585-33-9
lithium dimethylamide

: 1235259-89-8
[(p-tolyl)3(germanium)(NMe₂)]

Guidance literature:: In benzene; Schlenk, glove box technique, under N2; suspn. of LiNMe2 (5.49 mmol) added to soln. of Ge complex (5.117 mmol), stirred for 18 h; filtered, volatiles removed in vac., distilled in vac.; elem. anal.;
DOI:10.1016/j.jorganchem.2010.04.015

Reference yield:

: 58436-48-9
tri(p-tolyl)chlorogermane

: 926312-91-6
tert-Bu₂MeSiGe(p-tolyl)2Cl

Guidance literature:: Multi-step reaction with 3 steps

1: diethyl ether

2: tetrahydrofuran; diethyl ether; hexane

3: CF₃SO₃H / dichloromethane

With CF₃SO₃H; In tetrahydrofuran; diethyl ether; hexane; dichloromethane;
DOI:10.1016/j.jorganchem.2006.03.049