azelaic bishydroxamic acid

Base Information

• Chemical Name: azelaic bishydroxamic acid
• CAS No.: 18992-11-5
• Molecular Formula: C₉H₁₈N₂O₄
• Molecular Weight: 218.253
• Hs Code.: 2924199090
• Mol file: 18992-11-5.mol

Synonyms:Azelahydroxamicacid (6CI,8CI); Nonanediamide, N,N'-dihydroxy- (9CI); Azeladihydroxamic acid;Azelahydroximic acid; Azelaic bishydroxamic acid; Azelaoyl bis(hydroxamicacid); NSC 611775

Chemical Property of azelaic bishydroxamic acid

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 105.64000
• Density: 1.186g/cm³
• LogP: 2.40850

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of azelaic bishydroxamic acid

There total 2 articles about azelaic bishydroxamic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

azelaic acid (123-99-9,26776-28-3) → azelaic bishydroxamic acid (18992-11-5)

Guidance literature:

With hydroxylamine hydrochloride; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; triethylamine; In N,N-dimethyl-formamide; at 20 ℃; for 12h;

DOI:10.1016/S0006-2952(97)00016-6

Reference yield:

1,9-Di-imidazol-1-yl-nonane-1,9-dione (122236-59-3) → azelaic bishydroxamic acid (18992-11-5)

Guidance literature:

With hydroxylamine; In methanol; for 48h; Yield given; Ambient temperature;

upstream raw materials:

1,9-Di-imidazol-1-yl-nonane-1,9-dione

azelaic acid

Refernces

• 1、 Brown, David A.,Coogan, Raymond A.,Fitzpatrick, Noel J.,Glass, William K.,Abukshima, Dau E.,Shiels, Loreto,Ahlgren, Markku,Smolander, Kimmo,Pakkanen, Tuula T.,Pakkanen, Tapani A.,Peraekylae, Mikael. "Conformational behaviour of hydroxamic acids: Ab initio and structural studies". . p. 2673 - 2679. Retrieved 1996.