2(1H)-Pyridinone, 4-hydroxy-6-methyl-1-(2-pyridinylmethyl)- (9CI)

Base Information

Chemical Name:2(1H)-Pyridinone, 4-hydroxy-6-methyl-1-(2-pyridinylmethyl)- (9CI)
CAS No.:586378-69-0
Molecular Formula:C12H12N2O2
Molecular Weight:216.23600
Hs Code.:
Mol file:586378-69-0.mol

Synonyms:4-hydroxy-6-methyl-1-pyridin-2-ylmethyl-1H-pyridin-2-one;

Suppliers and Price of 2(1H)-Pyridinone, 4-hydroxy-6-methyl-1-(2-pyridinylmethyl)- (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 2 raw suppliers

Chemical Property of 2(1H)-Pyridinone, 4-hydroxy-6-methyl-1-(2-pyridinylmethyl)- (9CI)

Chemical Property:

PSA：55.12000
LogP:1.30560

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2(1H)-Pyridinone, 4-hydroxy-6-methyl-1-(2-pyridinylmethyl)- (9CI)

There total 2 articles about 2(1H)-Pyridinone, 4-hydroxy-6-methyl-1-(2-pyridinylmethyl)- (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 3731-51-9
2-(Aminomethyl)pyridine

: 675-10-5
4-hydroxy-6-methyl-2-pyron

: 586378-69-0
4-hydroxy-6-methyl-1-(pyridin-2-ylmethyl)pyridin-2(1H)-one

Guidance literature:: In water; for 2.5h; Heating / reflux;

Reference yield:

: 586378-69-0
4-hydroxy-6-methyl-1-(pyridin-2-ylmethyl)pyridin-2(1H)-one

Guidance literature:

Reference yield:

: 586378-69-0
4-hydroxy-6-methyl-1-(pyridin-2-ylmethyl)pyridin-2(1H)-one

: 636581-73-2
2-amino-5-(5-methyl-3-oxo-4-pyridin-2ylmethyl-cyclohexa-1,5-dienyl)-3-nitro-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / DMF (N,N-dimethyl-formamide) / 20 °C

2: sodium carbonate / bis-triphenylphosphine-palladium(II) chloride / 1,2-dimethoxyethane / 3 h / Heating / reflux

With sodium carbonate; triethylamine; bis-triphenylphosphine-palladium(II) chloride; In DMF (N,N-dimethyl-formamide); 1,2-dimethoxyethane;