(7aR,8aβ,11aβ,11bα,11cβ)-8β-Ethyltetradecahydro-11β-methylfuro[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10-one

Base Information

• Chemical Name: (7aR,8aβ,11aβ,11bα,11cβ)-8β-Ethyltetradecahydro-11β-methylfuro[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10-one
• CAS No.: 16625-37-9
• Molecular Formula: C₁₇H₂₇NO₂
• Molecular Weight: 277.407
• Mol file: 16625-37-9.mol

Synonyms:Stenine(8CI); (-)-Stenine; 2-Des(tetrahydro-4-methyl-5-oxo-2-furanyl)tuberostemonine;Furo[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10(2H)-one,8-ethyldodecahydro-11-methyl-, [7aR-(7aa,8a,8aa,11a,11aa,11bb,11ca)]-; Stenin; [7aR-(7aa,8a,8aa,11a,11aa,11bb,11ca)]-8-Ethyldodecahydro-11-methylfuro[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10(2H)-one

Chemical Property of (7aR,8aβ,11aβ,11bα,11cβ)-8β-Ethyltetradecahydro-11β-methylfuro[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10-one

Chemical Property:

• Vapor Pressure: 4.38E-07mmHg at 25°C
• Boiling Point: 414.6°Cat760mmHg
• Flash Point: 146.3°C
• PSA: 29.54000
• Density: 1.12g/cm³
• LogP: 2.63240

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (7aR,8aβ,11aβ,11bα,11cβ)-8β-Ethyltetradecahydro-11β-methylfuro[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10-one

There total 108 articles about (7aR,8aβ,11aβ,11bα,11cβ)-8β-Ethyltetradecahydro-11β-methylfuro[2,3-h]pyrrolo[3,2,1-jk][1]benzazepin-10-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

(+/-)-4-thiostenine → (+/-)-stenine (16625-37-9,130760-62-2)

Guidance literature:

With nickel; In ethanol; at 20 ℃; for 0.5h;

DOI:10.1021/ja055629m

Reference yield: 80.0%

C19H27NO2S3 (130796-98-4) → (+/-)-stenine (16625-37-9,130760-62-2)

Guidance literature:

With ethanol; W-2 Raney nickel; for 1h; Heating;

DOI:10.1021/jo00067a015

Reference yield: 78.0%

(-)-4-thiostenine (808470-75-9) → stenine (16625-37-9)

Guidance literature:

With nickel; In ethanol; at 21 ℃; for 0.5h;

DOI:10.1021/ja00150a010

upstream raw materials:

(-)-4-thiostenine

(1S,3aS,4R,5R,5aR,8aR,8bS)-4-Ethyl-5-(4-hydroxy-butyl)-1-methyl-2-oxo-decahydro-furo[3,2-e]indole-6-carboxylic acid methyl ester

(1S,3aS,4R,5R,5aR,8aR,8bS)-4-Ethyl-5-(4-iodo-butyl)-1-methyl-2-oxo-decahydro-furo[3,2-e]indole-6-carboxylic acid methyl ester

(1R,2R,4aS,8aR)-2-[4-(4-Methoxy-benzyloxy)-butyl]-6-oxo-1,2,4a,5,6,7,8,8a-octahydro-naphthalene-1-carbaldehyde

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