1-(furan-2-yl)-2-(methylsulfinyl)ethanone

Base Information

• Chemical Name: 1-(furan-2-yl)-2-(methylsulfinyl)ethanone
• CAS No.: 2891-96-5
• Molecular Formula: C7H8 O3 S
• Molecular Weight: 172.2016
• Mol file: 2891-96-5.mol

Synonyms:Ketone,2-furyl (methylsulfinyl)methyl (7CI,8CI); (Methylsulfinyl)methyl 2-furyl ketone

Chemical Property of 1-(furan-2-yl)-2-(methylsulfinyl)ethanone

Chemical Property:

• Vapor Pressure: 1.43E-06mmHg at 25°C
• Boiling Point: 398.9°Cat760mmHg
• Flash Point: 195°C
• PSA: 66.49000
• Density: 1.326g/cm³
• LogP: 1.70650

Purity/Quality:

1-(2-FURANYL)-2-(METHYLSULFINYL)ETHANONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(furan-2-yl)-2-(methylsulfinyl)ethanone

There total 3 articles about 1-(furan-2-yl)-2-(methylsulfinyl)ethanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

Ethyl 2-furoate (614-99-3) + dimethyl sulfoxide (67-68-5,8070-53-9) → (methylsulphinyl)methyl 2-furyl ketone (2891-96-5)

Guidance literature:

With potassium tert-butylate; In tert-butyl alcohol;

DOI:10.1016/0040-4020(89)80147-4

Reference yield:

→ (methylsulphinyl)methyl 2-furyl ketone (2891-96-5)

Guidance literature:

Furan-2-carbonsaeureaethylester, Methylsulfinylcarbanion in DMSO/ THF;

DOI:10.1021/ja01062a040

Reference yield:

→ (methylsulphinyl)methyl 2-furyl ketone (2891-96-5) + Methyl 3-Benzyloxy-3-methyl-2-oxobutyl Sulfoxide (109991-42-6)

Guidance literature:

upstream raw materials:

Ethyl 2-furoate

dimethyl sulfoxide