Hexanoic acid, 6-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2-[(1R)-1-[[(phen ylmethoxy)carbonyl]amino]ethyl]-, 1,1-dimethylethyl ester, (2S)-

Base Information

Chemical Name:Hexanoic acid, 6-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2-[(1R)-1-[[(phen ylmethoxy)carbonyl]amino]ethyl]-, 1,1-dimethylethyl ester, (2S)-
CAS No.:587840-67-3
Molecular Formula:C₃₂H₄₆N₂O₆
Molecular Weight:554.727
Hs Code.:

Hexanoic acid,
6-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2-[(1R)-1-[[(phen
ylmethoxy)carbonyl]amino]ethyl]-, 1,1-dimethylethyl ester, (2S)-

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Chemical Property of Hexanoic acid, 6-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2-[(1R)-1-[[(phen ylmethoxy)carbonyl]amino]ethyl]-, 1,1-dimethylethyl ester, (2S)-

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Technology Process of Hexanoic acid, 6-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2-[(1R)-1-[[(phen ylmethoxy)carbonyl]amino]ethyl]-, 1,1-dimethylethyl ester, (2S)-

There total 2 articles about Hexanoic acid, 6-[[(1,1-dimethylethoxy)carbonyl](phenylmethyl)amino]-2-[(1R)-1-[[(phen ylmethoxy)carbonyl]amino]ethyl]-, 1,1-dimethylethyl ester, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 13139-17-8
N-(Benzyloxycarbonyloxy)succinimide

: 2-(1-amino-ethyl)-6-(benzyl-tert-butoxycarbonyl-amino)-hexanoic acid tert-butyl ester

: 587840-67-3
6-(benzyl-tert-butoxycarbonyl-amino)-2-(1-benzyloxycarbonylamino-ethyl)-hexanoic acid tert-butyl ester

Guidance literature:: With sodium hydrogencarbonate; In water; acetone; at 20 ℃;
DOI:10.1021/jo034583h

Reference yield:

: 2-[4-(benzyl-tert-butoxycarbonyl-amino)-butyl]-but-2-enoic acid tert-butyl ester

: 587840-67-3
6-(benzyl-tert-butoxycarbonyl-amino)-2-(1-benzyloxycarbonylamino-ethyl)-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: toluene

1.2: HCOONH₄ / 10 percent Pd-C / 2-methyl-propan-2-ol / Heating

2.1: NaHCO₃ / acetone; H₂O / 20 °C

With sodium hydrogencarbonate; In water; acetone; toluene;
DOI:10.1021/jo034583h