TETRAKIS(DIETHYLAMINO)DIPHOSPHANE

Base Information

• Chemical Name: TETRAKIS(DIETHYLAMINO)DIPHOSPHANE
• CAS No.: 62591-87-1
• Molecular Formula: C₁₆H₄₀N₄P₂
• Molecular Weight: 350.468
• Mol file: 62591-87-1.mol

Synonyms:Hypodiphosphoroustetraamide, octaethyl- (9CI)

Chemical Property of TETRAKIS(DIETHYLAMINO)DIPHOSPHANE

Chemical Property:

• Boiling Point: 390.7oC at 760 mmHg
• Flash Point: 190.1oC
• PSA: 40.14000
• LogP: 4.89240

Purity/Quality:

TETRAKIS(DIETHYLAMINO)DIPHOSPHANE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TETRAKIS(DIETHYLAMINO)DIPHOSPHANE

There total 2 articles about TETRAKIS(DIETHYLAMINO)DIPHOSPHANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(Et2N)2PP(SiMe3)Li → (Et2N)2PP(SiMe3)2 + tetrakis(diethylamino)diphosphane (62591-87-1)

Guidance literature:

With zirconocene dichloride; In pentane; at -40 - 20 ℃; for 1h;

DOI:10.1039/c0dt01040e

Reference yield:

(Et2N)2PP(SiMe3)Li → (Et2N)2PP(SiMe3)2 + tetrakis(diethylamino)diphosphane (62591-87-1) + 1,3-bis(diethylamino)-2,4-bis(trimethylsilyl)-1,2,3,4-tetraphosphetane (1279124-37-6) + C19H49N4P5Si (1279124-46-7)

Guidance literature:

With cyclopentadienylzirconium trichloride; at -40 - 20 ℃; for 1h;

DOI:10.1039/c0dt01040e

Refernces