5-methyl-6-phenylimidazo[2,1-b][1,3]thiazole

Base Information

• Chemical Name: 5-methyl-6-phenylimidazo[2,1-b][1,3]thiazole
• CAS No.: 51226-38-1
• Molecular Formula: C12H10 N2 S
• Molecular Weight: 214.2862
• Mol file: 51226-38-1.mol

Synonyms:NSC 315211

Chemical Property of 5-methyl-6-phenylimidazo[2,1-b][1,3]thiazole

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.26g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-methyl-6-phenylimidazo[2,1-b][1,3]thiazole

There total 4 articles about 5-methyl-6-phenylimidazo[2,1-b][1,3]thiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

6-phenylimidazo<2,1-b>thiazole-5-acetic acid → 5-methyl-6-phenylimidazo[2,1-b]thiazole (51226-38-1)

Guidance literature:

In 1-methyl-pyrrolidin-2-one; at 220 - 240 ℃; for 0.333333h; Sealed tube; Microwave irradiation;

DOI:10.1021/acs.orglett.8b00190

Reference yield: 46.0%

6-phenylimidazo<2,1-b>thiazole-5-acetic acid → 5-methyl-6-phenylimidazo[2,1-b]thiazole (51226-38-1) + N,N-dimethyl-2-(6-phenylimidazo[2,1-b]thiazol-5-yl)acetamide

Guidance literature:

In N,N-dimethyl acetamide; at 200 - 220 ℃; for 1.33333h; Sealed tube; Microwave irradiation;

DOI:10.1021/acs.orglett.8b00190

Reference yield:

2-thiazolylamine (96-50-4) + C15H12N2O8S → 5-methyl-6-phenylimidazo[2,1-b]thiazole (51226-38-1)

Guidance literature:

With sodium carbonate; at 80 ℃; for 0.5h;

DOI:10.1002/jccs.201190103

upstream raw materials:

2-thiazolylamine

1-phenyl-propan-1-one

Downstream raw materials:

6-phenylimidazo[2,1-b]thiazole-5-carbaldehyde

5-methyl-6-(4-nitroso-phenyl)-imidazo[2,1-b]thiazole

N-(5-methyl-6-phenyl-imidazo[2,1-b]thiazol-2-yl)-hydrazine-N,N'-dicarboxylic acid diethyl ester

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