4-Hexenal, 3-[(4-methoxyphenoxy)methyl]-, (3S,4E)-

Base Information

Chemical Name:4-Hexenal, 3-[(4-methoxyphenoxy)methyl]-, (3S,4E)-
CAS No.:592508-24-2
Molecular Formula:C14H18O3
Molecular Weight:234.295
Hs Code.:

Synonyms:

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Chemical Property of 4-Hexenal, 3-[(4-methoxyphenoxy)methyl]-, (3S,4E)-

Chemical Property:

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Technology Process of 4-Hexenal, 3-[(4-methoxyphenoxy)methyl]-, (3S,4E)-

There total 6 articles about 4-Hexenal, 3-[(4-methoxyphenoxy)methyl]-, (3S,4E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (E)-(S)-3-(4-Methoxy-phenoxymethyl)-hex-4-en-1-ol

: 592508-24-2
(E)-(S)-3-(4-Methoxy-phenoxymethyl)-hex-4-enal

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃;
DOI:10.1016/S0040-4039(03)00749-4

Reference yield:

: 189630-90-8
(4S,2E)-4-[(tert-butyldiphenylsilyl)oxy]pent-2-en-1-ol

: 592508-24-2
(E)-(S)-3-(4-Methoxy-phenoxymethyl)-hex-4-enal

Guidance literature:: Multi-step reaction with 5 steps

1: 89 percent / DEAD; PPh₃ / tetrahydrofuran / 20 °C

2: 92 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

3: 98 percent / decahydronaphthalene / Heating

4: lithium triethylborohydride / tetrahydrofuran / -78 - 20 °C

5: (COCl)2; DMSO; NEt₃ / CH₂Cl₂ / -78 °C

With oxalyl dichloride; tetrabutyl ammonium fluoride; lithium triethylborohydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; decalin; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 1: Mitsunobu reaction / 3: Claisen rearrangement / 5: Swern oxidation;
DOI:10.1016/S0040-4039(03)00749-4

Reference yield:

: 203387-35-3
(E)-(S)-4-(tert-butyl-diphenyl-silanyloxy)-pent-2-enoic acid ethyl ester

: 592508-24-2
(E)-(S)-3-(4-Methoxy-phenoxymethyl)-hex-4-enal

Guidance literature:: Multi-step reaction with 6 steps

1: di-iso-butylaluminum hydride / tetrahydrofuran / -78 - 0 °C

2: 89 percent / DEAD; PPh₃ / tetrahydrofuran / 20 °C

3: 92 percent / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

4: 98 percent / decahydronaphthalene / Heating

5: lithium triethylborohydride / tetrahydrofuran / -78 - 20 °C

6: (COCl)2; DMSO; NEt₃ / CH₂Cl₂ / -78 °C

With oxalyl dichloride; diisobutylaluminum hydride; tetrabutyl ammonium fluoride; lithium triethylborohydride; dimethyl sulfoxide; triethylamine; triphenylphosphine; decalin; diethylazodicarboxylate; In tetrahydrofuran; dichloromethane; 2: Mitsunobu reaction / 4: Claisen rearrangement / 6: Swern oxidation;
DOI:10.1016/S0040-4039(03)00749-4