4-Methyl-1-morpholinocyclohexene

Base Information

Chemical Name:4-Methyl-1-morpholinocyclohexene
CAS No.:5601-45-6
Molecular Formula:C11H19NO
Molecular Weight:181.278
Hs Code.:
NSC Number:203399
DSSTox Substance ID:DTXSID00308396
Nikkaji Number:J101.909K
Mol file:5601-45-6.mol

Synonyms:4-Methyl-1-morpholinocyclohexene;5601-45-6;Morpholine, 4-(4-methyl-1-cyclohexen-1-yl)-;NSC203399;4-(4-Methyl-cyclohex-1-enyl)-morpholine;SCHEMBL412859;DTXSID00308396;AKOS006318844;NSC-203399;4-(4-Methyl-1-cyclohexen-1-yl)morpholine #

Suppliers and Price of 4-Methyl-1-morpholinocyclohexene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 4-Methyl-1-morpholinocyclohexene

Chemical Property:

Vapor Pressure:0.00297mmHg at 25°C
Boiling Point:284.5°Cat760mmHg
Flash Point:83.8°C
PSA：12.47000
Density:1.007g/cm³
LogP:1.96040
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:181.146664230
Heavy Atom Count:13
Complexity:194

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCC(=CC1)N2CCOCC2

Technology Process of 4-Methyl-1-morpholinocyclohexene

There total 2 articles about 4-Methyl-1-morpholinocyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 110-91-8,99108-56-2
morpholine

: 589-92-4
1-methylcyclohexan-4-one

: 5601-45-6
4-(4-methylcyclohex-1-en-1-yl)morpholine

Guidance literature:: With toluene-4-sulfonic acid; In toluene; for 4h; Heating;
DOI:10.1016/j.tet.2005.01.036

Reference yield:

: 5601-45-6
4-(4-methylcyclohex-1-en-1-yl)morpholine

Guidance literature:: 4-Methylcyclohexanon/Morpholin/Toluol/p-Toluolsulfonsaeure;

Reference yield: 92.0%

: 5601-45-6
4-(4-methylcyclohex-1-en-1-yl)morpholine

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: C₁₉H₂₁O₂P

Guidance literature:: 4-(4-methylcyclohex-1-en-1-yl)morpholine; chloro-diphenylphosphine; With triethylamine; In acetonitrile; at 0 - 25 ℃; for 2h; Inert atmosphere;

With dimethyl sulfoxide; In acetonitrile; for 2h; Reflux;

With hydrogenchloride; In water; acetonitrile; at 0 - 25 ℃; for 12h;
DOI:10.1002/cbdv.202000217