7,8,14-Trioxa-2,12-diazahexadecanoic acid, 11-[(1,1-dimethylethoxy)carbonyl]-15,15-dimethyl-6,9,13-trioxo-3-[(phen ylmethoxy)carbonyl]-, phenylmethyl ester, (3S,11S)-

Base Information

Chemical Name:7,8,14-Trioxa-2,12-diazahexadecanoic acid, 11-[(1,1-dimethylethoxy)carbonyl]-15,15-dimethyl-6,9,13-trioxo-3-[(phen ylmethoxy)carbonyl]-, phenylmethyl ester, (3S,11S)-
CAS No.:592532-10-0
Molecular Formula:C33H42N2O12
Molecular Weight:658.703
Hs Code.:

7,8,14-Trioxa-2,12-diazahexadecanoic acid,
11-[(1,1-dimethylethoxy)carbonyl]-15,15-dimethyl-6,9,13-trioxo-3-[(phen
ylmethoxy)carbonyl]-, phenylmethyl ester, (3S,11S)-

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Chemical Property of 7,8,14-Trioxa-2,12-diazahexadecanoic acid, 11-[(1,1-dimethylethoxy)carbonyl]-15,15-dimethyl-6,9,13-trioxo-3-[(phen ylmethoxy)carbonyl]-, phenylmethyl ester, (3S,11S)-

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Technology Process of 7,8,14-Trioxa-2,12-diazahexadecanoic acid, 11-[(1,1-dimethylethoxy)carbonyl]-15,15-dimethyl-6,9,13-trioxo-3-[(phen ylmethoxy)carbonyl]-, phenylmethyl ester, (3S,11S)-

There total 3 articles about 7,8,14-Trioxa-2,12-diazahexadecanoic acid, 11-[(1,1-dimethylethoxy)carbonyl]-15,15-dimethyl-6,9,13-trioxo-3-[(phen ylmethoxy)carbonyl]-, phenylmethyl ester, (3S,11S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 34582-32-6
N-tert-butoxycarbonyl aspartic acid tert-butyl ester

: 592532-04-2
(S)-2-Benzyloxycarbonylamino-4-hydroperoxycarbonyl-butyric acid benzyl ester

: 592532-10-0
4-(4-benzyloxycarbonyl-4-benzyloxycarbonylamino-butyrylperoxy)-2-tert-butoxycarbonylamino-4-oxo-butyric acid tert-butyl ester

Guidance literature:: With dicyclohexyl-carbodiimide; In dichloromethane; at 0 - 20 ℃;
DOI:10.1021/ol035125y

Reference yield:

: 3705-42-8
Cbz-(L)-Glu-OBn

: 592532-10-0
4-(4-benzyloxycarbonyl-4-benzyloxycarbonylamino-butyrylperoxy)-2-tert-butoxycarbonylamino-4-oxo-butyric acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / DCC; DMAP / CH₂Cl₂ / -20 - 20 °C

2: 94 percent / aq. TFA / CHCl₃ / 0.25 h / 20 °C

3: 89 percent / DCC / CH₂Cl₂ / 0 - 20 °C

With dmap; dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1021/ol035125y

Reference yield:

: 592532-02-0
(S)-2-Benzyloxycarbonylamino-4-(1-methoxy-1-methyl-ethylperoxycarbonyl)-butyric acid benzyl ester

: 592532-10-0
4-(4-benzyloxycarbonyl-4-benzyloxycarbonylamino-butyrylperoxy)-2-tert-butoxycarbonylamino-4-oxo-butyric acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / aq. TFA / CHCl₃ / 0.25 h / 20 °C

2: 89 percent / DCC / CH₂Cl₂ / 0 - 20 °C

With dicyclohexyl-carbodiimide; trifluoroacetic acid; In dichloromethane; chloroform;
DOI:10.1021/ol035125y