methyl 2-{[(5-bromofuran-2-yl)carbonyl]amino}benzoate

Base Information

Chemical Name:methyl 2-{[(5-bromofuran-2-yl)carbonyl]amino}benzoate
CAS No.:6410-50-0
Molecular Formula:C₁₁H₁₆N₆O₆
Molecular Weight:328.285
Hs Code.:

Synonyms:Mannopyranoside,methyl 2,3-diazido-2,3-dideoxy-, diacetate (7CI); Mannopyranoside, methyl 2,3-diazido-2,3-dideoxy-,diacetate (ester), a-D- (8CI)

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-{[(5-bromofuran-2-yl)carbonyl]amino}benzoate

Chemical Property:

Vapor Pressure:5.42E-05mmHg at 25°C
Boiling Point:347.3°Cat760mmHg
Flash Point:163.9°C
Density:1.579g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of methyl 2-{[(5-bromofuran-2-yl)carbonyl]amino}benzoate

There total 3 articles about methyl 2-{[(5-bromofuran-2-yl)carbonyl]amino}benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 287719-32-8
methyl 2,3-diazido-2,3-dideoxy-α-D-mannopyranoside

: 108-24-7
acetic anhydride

: 6410-50-0
methyl 4,6-di-O-acetyl-2,3-diazido-2,3-dideoxy-α-D-mannopyranoside

Guidance literature:: With pyridine;
DOI:10.1021/ol0058893

Reference yield:

: 287719-31-7
methyl 2,3-diazido-4,6-O-benzylidene-2,3-dideoxy-α-D-mannopyranoside

: 6410-50-0
methyl 4,6-di-O-acetyl-2,3-diazido-2,3-dideoxy-α-D-mannopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / AcOH / H₂O

2: 91 percent / pyridine

With pyridine; acetic acid; In water; 1: Hydrolysis / 2: Acetylation;
DOI:10.1021/ol0058893