Technology Process of Molybdenum, (eta6-benzene)(eta6-5-(1-methylethylidene-1,3-cyclopentadiene)-
There total 1 articles about Molybdenum, (eta6-benzene)(eta6-5-(1-methylethylidene-1,3-cyclopentadiene)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
In
toluene;
a soln. of Mo(C6H6)2 in toluene was treated with the fulvene, mixt. wasstirred at 50°C for 2 d; exclusion of moisture and O2;; the solvent was removed under reduced pressure, mixt. was extd. with MeOH, the soln. was concd., cooled to -20°C for 12 h, ppt. was collected, washed with cold MeOH; elem. anal.;