2-Iodo-1,5-dimethyl-3-nitrobenzene

Base Information

Chemical Name:2-Iodo-1,5-dimethyl-3-nitrobenzene
CAS No.:593255-20-0
Molecular Formula:C8H8INO2
Molecular Weight:277.062
Hs Code.:2904909090
DSSTox Substance ID:DTXSID20556039
Wikidata:Q82437507
Mol file:593255-20-0.mol

Synonyms:2-Iodo-1,5-dimethyl-3-nitrobenzene;593255-20-0;1-Iodo-2,4-dimethyl-6-nitrobenzene;SCHEMBL12434986;DTXSID20556039;MFCD19704776;AKOS025295506;1-Iodo-2,4-dimethyl-6-nitrobenzene, 97%;CS-0241841;G68378;A869220;EN300-23909281

Suppliers and Price of 2-Iodo-1,5-dimethyl-3-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Sigma-Aldrich
1-Iodo-2,4-dimethyl-6-nitrobenzene 97%
5g
$ 87.40

Alichem
1,5-Dimethyl-2-iodo-3-nitrobenzene
1g
$ 1534.70

Alichem
1,5-Dimethyl-2-iodo-3-nitrobenzene
500mg
$ 782.40

Alichem
1,5-Dimethyl-2-iodo-3-nitrobenzene
250mg
$ 489.60

AK Scientific
1-Iodo-2,4-dimethyl-6-nitrobenzene
5g
$ 160.00

Total 5 raw suppliers

Chemical Property of 2-Iodo-1,5-dimethyl-3-nitrobenzene

Chemical Property:

Melting Point:102-107°C
Boiling Point:320.0±30.0 °C(Predicted)
PSA：45.82000
Density:1.777±0.06 g/cm3(Predicted)
LogP:3.33940
Storage Temp.:2-8°C
XLogP3:3.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:276.95998
Heavy Atom Count:12
Complexity:180

Purity/Quality:

97% ^*data from raw suppliers

1-Iodo-2,4-dimethyl-6-nitrobenzene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC(=C(C(=C1)[N+](=O)[O-])I)C

Technology Process of 2-Iodo-1,5-dimethyl-3-nitrobenzene

There total 3 articles about 2-Iodo-1,5-dimethyl-3-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 1635-84-3
2,4-Dimethyl-6-nitroanilin

: 593255-20-0
2-iodo-3,5-dimethyl-1-nitrobenzene

Guidance literature:: 2,4-Dimethyl-6-nitroanilin; With sulfuric acid; sodium nitrite; In acetic acid; at 15 - 75 ℃;

With urea; potassium iodide;
DOI:10.1016/S0957-4166(03)00217-9

Reference yield:

: 95-68-1
2,4-Xylidine

: 593255-20-0
2-iodo-3,5-dimethyl-1-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1.1: 86 percent / 96 percent HNO₃; Ac₂O / 1.17 h / 7 °C

2.1: NaNO₂; conc. H₂SO₄ / acetic acid / 15 - 75 °C

2.2: 69 percent / aq. KI; urea

With sulfuric acid; nitric acid; acetic anhydride; sodium nitrite; In acetic acid;
DOI:10.1016/S0957-4166(03)00217-9