Cyclohexanamine, 2-methyl-1-phenyl-

Base Information

Chemical Name:Cyclohexanamine, 2-methyl-1-phenyl-
CAS No.:59397-27-2
Molecular Formula:C13H19N
Molecular Weight:189.301
Hs Code.:
DSSTox Substance ID:DTXSID30483660

Synonyms:Cyclohexanamine, 2-methyl-1-phenyl-;59397-27-2;DTXSID30483660

Suppliers and Price of Cyclohexanamine, 2-methyl-1-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Cyclohexanamine, 2-methyl-1-phenyl-

Chemical Property:

XLogP3:2.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:189.151749610
Heavy Atom Count:14
Complexity:184

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1CCCCC1(C2=CC=CC=C2)N

Technology Process of Cyclohexanamine, 2-methyl-1-phenyl-

There total 7 articles about Cyclohexanamine, 2-methyl-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 66021-72-5
(1-Azido-2-methyl-cyclohexyl)-benzene

: 59397-27-2
2-Methyl-1-phenyl-cyclohexylamine

Guidance literature:: With Raney nickel; In isopropyl alcohol; at 60 - 70 ℃;
DOI:10.15227/orgsyn.060.0104

Reference yield:

: 15036-22-3
1-phenyl-2-methylcyclohexanol

: 125801-98-1,129329-46-0,58283-39-9,58283-40-2,59397-27-2,125801-96-9
cis-Ph/Me 1-(1-phenyl-2-methylcyclohexyl)amine

Guidance literature:: Multi-step reaction with 2 steps

1: sodium azide, concd. H₂SO₄ / CHCl₃ / 6 h / 0 °C

2: LAH / diethyl ether / 1 h / Heating

With lithium aluminium tetrahydride; sodium azide; sulfuric acid; In diethyl ether; chloroform;
DOI:10.1021/jm00112a041

Reference yield:

: phenylmagnesium bromide

: 125801-98-1,129329-46-0,58283-39-9,58283-40-2,59397-27-2,125801-96-9
cis-Ph/Me 1-(1-phenyl-2-methylcyclohexyl)amine

Guidance literature:: Multi-step reaction with 3 steps

1: tetrahydrofuran / 0.33 h

2: NaN₃, CF₃COOH / CHCl₃ / Ambient temperature

3: LiAlH₄ / diethyl ether / 3 h / Heating

With lithium aluminium tetrahydride; sodium azide; trifluoroacetic acid; In tetrahydrofuran; diethyl ether; chloroform;
DOI:10.1021/jm00167a027