2,4,4-Trimethylcyclohexene-1-carbaldehyde

Base Information

• Chemical Name: 2,4,4-Trimethylcyclohexene-1-carbaldehyde
• CAS No.: 5939-87-7
• Molecular Formula: C10H16O
• Molecular Weight: 152.236
• Mol file: 5939-87-7.mol

Synonyms:β-cyclolavandulal;2,4,4-trimethyl-cyclohex-1-enecarbaldehyde;β-cyclolavandulol;2,4,4-Trimethyl-cyclohex-1-encarbaldehyd;

Chemical Property of 2,4,4-Trimethylcyclohexene-1-carbaldehyde

Chemical Property:

• Boiling Point: 88 - 91 °C (7.9508 mmHg)
• PSA: 17.07000
• LogP: 2.71190

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2,4,4-Trimethylcyclohexene-1-carbaldehyde

There total 17 articles about 2,4,4-Trimethylcyclohexene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

(2,4,4-trimethyl-1-cyclohexen-1-yl)methanol (103985-40-6) → (2,4,4-trimethyl-1-cyclohexene)carbaldehyde (5939-87-7)

Guidance literature:

With pyridinium chlorochromate; In dichloromethane; for 0.25h; Ambient temperature;

Reference yield: 95.0%

2,4,4-trimethyl-2-cyclohexenylidenemethyl methyl ether → (2,4,4-trimethyl-1-cyclohexene)carbaldehyde (5939-87-7)

Guidance literature:

With hydrogenchloride; In diethyl ether; water; at 20 ℃; for 2h;

Reference yield:

2,4,4-trimethyl-2-cyclohexenylidenemethyl methyl ether → (2,4,4-trimethyl-2-cyclohexene)formaldehyde + (2,4,4-trimethyl-1-cyclohexene)carbaldehyde (5939-87-7)

Guidance literature:

With hydrogenchloride; In diethyl ether; water; at 20 ℃; for 2h;

upstream raw materials:

(2,4,4-trimethyl-1-cyclohexen-1-yl)methanol

(+/-)-5.5-dimethyl-2-hydroxymethyl-1-methylene-cyclohexane

2-isobutoxymethylene-5,5-dimethyl-cyclohexanone

aluminum isopropoxide

Downstream raw materials:

(2,4,4-trimethyl-1-cyclohexen-1-yl)methanol

methyl β-cyclolavandulate

(2,4,4-trimethyl-1-cyclohexen-1-yl)carboxylic acid

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