2-Ethylbicyclo[2.2.1]hept-5-ene-2-carboxamide

Base Information

• Chemical Name: 2-Ethylbicyclo[2.2.1]hept-5-ene-2-carboxamide
• CAS No.: 69365-83-9
• Molecular Formula: C10H15NO
• Molecular Weight: 165.2322
• DSSTox Substance ID: DTXSID50989139

Synonyms:2-ethylbicyclo[2.2.1]hept-5-ene-2-carboxamide;2-Norbornene-5-exo-carboxamide, 5-endo-ethyl-;69365-83-9;MLS002695116;5-endo-Ethyl-2-norbornene-5-exo-carboxamide;5-exo-Ethyl-2-norbornene-5-endo-carboxamide;2-Norbornene-5-endo-carboxamide, 5-exo-ethyl-;NCIOpen2_001343;SCHEMBL7110643;DTXSID50989139;HMS3079E03;NSC 92381;SMR001561028;2-Ethylbicyclo[2.2.1]hept-5-ene-2-carboximidic acid

Chemical Property of 2-Ethylbicyclo[2.2.1]hept-5-ene-2-carboxamide

Chemical Property:

• Vapor Pressure: 0.000539mmHg at 25°C
• Boiling Point: 312.1°Cat760mmHg
• Flash Point: 142.6°C
• Density: 1.08g/cm³
• XLogP3: 1.2
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 1
• Rotatable Bond Count: 2
• Exact Mass: 165.115364102
• Heavy Atom Count: 12
• Complexity: 246

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CCC1(CC2CC1C=C2)C(=O)N

Technology Process of 2-Ethylbicyclo[2.2.1]hept-5-ene-2-carboxamide

There total 6 articles about 2-Ethylbicyclo[2.2.1]hept-5-ene-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ (+/-)-2-ethyl-norborn-5-ene-2endo-carboxylic acid amide (69365-83-9,69365-84-0,91251-63-7)

Guidance literature:

With potassium hydroxide;

DOI:10.1021/ja01553a044

Reference yield:

(+/-)-2-ethyl-norborn-5-ene-2exo-carbonyl chloride → 5endo-Aethyl-5exo-carbamoyl-norbornen-(2) (69365-83-9,69365-84-0,91251-63-7)

Guidance literature:

With diethyl ether; ammonia;

DOI:10.1021/ja01553a044

Reference yield:

(+/-)-2-ethyl-norborn-5-ene-2endo-carbonitrile (28072-02-8,28072-05-1,72674-40-9) → (+/-)-2-ethyl-norborn-5-ene-2endo-carboxylic acid amide (69365-83-9,69365-84-0,91251-63-7) + (+/-)-2-ethyl-norborn-5-ene-2endo-carboxylic acid (73873-18-4)

Guidance literature:

With potassium hydroxide; ethylene glycol;

DOI:10.1021/ja01553a044

upstream raw materials:

(+/-)-2-ethyl-norborn-5-ene-2endo-carbonitrile

2-ethyl-acrylonitrile

cyclopenta-1,3-diene

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