17-Norkaur-15-ene-13-methanol

Base Information

• Chemical Name: 17-Norkaur-15-ene-13-methanol
• CAS No.: 20107-91-9
• Molecular Formula: C20H32O
• Molecular Weight: 288.47
• Mol file: 20107-91-9.mol

Synonyms:Diterpene mono-ol-B;Stach-15-en-17-ol;ent-beyer-15-en-17-ol;Stachenol B, Stachen-17-ol;Erythroxylol B;

Chemical Property of 17-Norkaur-15-ene-13-methanol

Chemical Property:

• PSA: 20.23000
• LogP: 4.94780

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 17-Norkaur-15-ene-13-methanol

There total 5 articles about 17-Norkaur-15-ene-13-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl ent-beyer-15-en-17-oate → ent-beyer-15-en-17-ol (20107-91-9)

Guidance literature:

With lithium aluminium tetrahydride;

DOI:10.1016/0031-9422(84)83032-0

Reference yield:

ent-beyer-15-en-17-oic acid → ent-beyer-15-en-17-ol (20107-91-9)

Guidance literature:

Multi-step reaction with 2 steps

2: LiAlH₄

With lithium aluminium tetrahydride;

DOI:10.1016/0031-9422(84)83032-0

Reference yield:

jativatriol (52591-20-5) → ent-beyer-15-en-17-ol (20107-91-9)

Guidance literature:

Multi-step reaction with 3 steps

1: Py

2: CrO₃, H₂SO₄

3: (i) N₂H₄*H₂O, triethylene glycol, (ii) KOH, (heating)

With pyridine; chromium(VI) oxide; sulfuric acid;

upstream raw materials:

17-Acetoxystach-15-en-1.12-dion

jativatriol

Stach-15-en-1α,12β,17-triol-17-acetat

Downstream raw materials:

Erythroxylol B-p-toluolsulfonat

(+)-hibaene