4,4'-Butylidenebis(2,6-xylenol)

Base Information

Chemical Name:4,4'-Butylidenebis(2,6-xylenol)
CAS No.:82209-87-8
Molecular Formula:C20H26 O2
Molecular Weight:298.425
Hs Code.:
European Community (EC) Number:279-921-7
DSSTox Substance ID:DTXSID10897408
Nikkaji Number:J118.411C
Wikidata:Q82873345
Mol file:82209-87-8.mol

Synonyms:82209-87-8;4,4'-Butylidenebis(2,6-xylenol);EINECS 279-921-7;SCHEMBL7202914;DTXSID10897408;JZTRTASDMYYCMP-UHFFFAOYSA-N;NS00093672

Suppliers and Price of 4,4'-Butylidenebis(2,6-xylenol)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 8 raw suppliers

Chemical Property of 4,4'-Butylidenebis(2,6-xylenol)

Chemical Property:

PSA：40.46000
LogP:5.26340
XLogP3:6
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:298.193280068
Heavy Atom Count:22
Complexity:289

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCCC(C1=CC(=C(C(=C1)C)O)C)C2=CC(=C(C(=C2)C)O)C

Technology Process of 4,4'-Butylidenebis(2,6-xylenol)

There total 3 articles about 4,4'-Butylidenebis(2,6-xylenol) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 123-72-8
butyraldehyde

: 82209-87-8
4,4'-butylidenebis(2,6-xylenol)

Guidance literature:: With hydrogenchloride; In Petroleum ether; at 27 ℃; for 4.25h;
DOI:10.1016/j.tet.2014.05.020

Reference yield:

: 95-48-7,77504-84-8
ortho-cresol

: 82209-87-8
4,4'-butylidenebis(2,6-xylenol)

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) SnCl₄, 2.) Raney Ni / 1.) CH₂Cl₂, room temp., 1 h, 2.) acetone, ethanol, room temp., 1 h

2: 1.) SnCl₄, 2.) Raney Ni / 1.) CH₂Cl₂, room temp., 1 h, 2.) acetone, ethanol, room temp., 1 h

With tin(IV) chloride; nickel;
DOI:10.1055/s-1982-30005

Reference yield:

: 576-26-1,25134-01-4
2.6-dimethylphenol

: 72653-47-5
α-chlorobutyl phenyl sulfide

: 6676-26-2
4-Butyl-2,6-dimethyl-phenol

: 82209-87-8
4,4'-butylidenebis(2,6-xylenol)

Guidance literature:: With tin(IV) chloride; nickel; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, room temp., 1 h, 2.) acetone, ethanol, room temp., 1 h;
DOI:10.1055/s-1982-30005