1,3,4-Thiadiazol-2-amine, 5-(2-methylphenyl)-

Base Information

Chemical Name:1,3,4-Thiadiazol-2-amine, 5-(2-methylphenyl)-
CAS No.:59565-54-7
Molecular Formula:C9H9N3S
Molecular Weight:191.257
Hs Code.:2934999090
Mol file:59565-54-7.mol

Synonyms:2-amino-5-o-tolyl-1,3,4-thiadiazole;5-o-tolyl-2-amino-1,3,4-thiadizole;

Suppliers and Price of 1,3,4-Thiadiazol-2-amine, 5-(2-methylphenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
2-Amino-5-(o-tolyl)-1,3,4-thiadiazole
100mg
$ 65.00

TRC
2-Amino-5-(o-tolyl)-1,3,4-thiadiazole
250mg
$ 125.00

Matrix Scientific
2-Amino-5-(o-tolyl)-1,3,4-thiadiazole
1g
$ 229.00

Matrix Scientific
2-Amino-5-(o-tolyl)-1,3,4-thiadiazole
500mg
$ 125.00

Crysdot
5-(o-Tolyl)-1,3,4-thiadiazol-2-amine 95+%
10g
$ 307.00

Crysdot
5-(o-Tolyl)-1,3,4-thiadiazol-2-amine 95+%
25g
$ 614.00

ChemBridge Corporation
5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine 95%
5 g
$ 133.00

American Custom Chemicals Corporation
5-(2-METHYLPHENYL)-1,3,4-THIADIAZOL-2-AMINE 95.00%
500MG
$ 762.30

Ambeed
5-(o-Tolyl)-1,3,4-thiadiazol-2-amine 95%
25g
$ 96.00

Ambeed
5-(o-Tolyl)-1,3,4-thiadiazol-2-amine 95%
10g
$ 46.00

Total 13 raw suppliers

Chemical Property of 1,3,4-Thiadiazol-2-amine, 5-(2-methylphenyl)-

Chemical Property:

Vapor Pressure:9.56E-06mmHg at 25°C
Boiling Point:372.5oC at 760 mmHg
Flash Point:179.1oC
PSA：80.04000
Density:1.281g/cm3
LogP:2.67690
Storage Temp.:under inert gas (nitrogen or Argon) at 2–8 °C

Purity/Quality:

97% ^*data from raw suppliers

2-Amino-5-(o-tolyl)-1,3,4-thiadiazole ^*data from reagent suppliers

Safty Information:

Pictogram(s): Xi
Hazard Codes:Xi,Xn
Statements: 22

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3,4-Thiadiazol-2-amine, 5-(2-methylphenyl)-

There total 5 articles about 1,3,4-Thiadiazol-2-amine, 5-(2-methylphenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 2290-65-5
trimethylsilyl isothiocyanate

: 7658-80-2
2-methylbenzohydrazide

: 59565-54-7
5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: trimethylsilyl isothiocyanate; 2-methylbenzohydrazide; In ethanol; Reflux;

With sulfuric acid; In ethanol; at 20 ℃;
DOI:10.1039/c3ra00159h

Reference yield: 73.0%

: 118-90-1
ortho-methylbenzoic acid

: 79-19-6
thiosemicarbazide

: 59565-54-7
5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: With trichlorophosphate; Reflux;
DOI:10.5012/bkcs.2010.31.8.2345

Reference yield:

: 5706-81-0
2'-methylbenzaldehyde-thiosemicarbazone

: 59565-54-7
5-(2-methylphenyl)-1,3,4-thiadiazol-2-amine

Guidance literature:: With iodosylbenzene; dihydrogen peroxide; acetic acid; In dimethyl sulfoxide; at 60 ℃; for 4h; Green chemistry;
DOI:10.1007/s10562-018-2541-y