Aminopeptidase N Inhibitor

Base Information

• Chemical Name: Aminopeptidase N Inhibitor
• CAS No.: 596108-59-7
• Molecular Formula: C17H10N2O8
• Molecular Weight: 370.275
• Mol file: 596108-59-7.mol

Synonyms:

Chemical Property of Aminopeptidase N Inhibitor

Chemical Property:

• PSA: 159.15000
• LogP: 3.94990

Purity/Quality:

≥95% ^*data from raw suppliers

AminopeptidaseNInhibitor >98% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Aminopeptidase N Inhibitor

There total 1 articles about Aminopeptidase N Inhibitor which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

8-allyl-3-nitro-2-(2-nitro-phenyl)-chromen-4-one (596108-47-3) → [3-nitro-2-(2-nitro-phenyl)-4-oxo-4H-chromen-8-yl]-acetic acid (596108-59-7)

Guidance literature:

With ruthenium trichloride; sodium periodate; In tetrachloromethane; acetonitrile; at 20 ℃; for 2h;

DOI:10.1021/jm021109f

Reference yield: 98.0%

chloromethyl methyl ether (107-30-2) + [3-nitro-2-(2-nitro-phenyl)-4-oxo-4H-chromen-8-yl]-acetic acid (596108-59-7) → [3-nitro-2-(2-nitro-phenyl)-4-oxo-4H-chromen-8-yl]-acetic acid methoxymethyl ester (596108-73-5)

Guidance literature:

With triethylamine; In acetonitrile; at 20 ℃; for 5h;

DOI:10.1021/jm021109f

Reference yield:

[3-nitro-2-(2-nitro-phenyl)-4-oxo-4H-chromen-8-yl]-acetic acid (596108-59-7) → 3-amino-2-(2-aminophenyl)-4-oxo-4H-1-benzopyran-8-acetic acid methoxymethyl ester (596108-77-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / triethylamine / acetonitrile / 5 h / 20 °C

2: 40 percent / H₂ / Pd/C / ethyl acetate / 16 h / 20 °C / 760 Torr

With hydrogen; triethylamine; palladium on activated charcoal; In ethyl acetate; acetonitrile;

DOI:10.1021/jm021109f

upstream raw materials:

8-allyl-3-nitro-2-(2-nitro-phenyl)-chromen-4-one

Downstream raw materials:

[3-nitro-2-(2-nitro-phenyl)-4-oxo-4H-chromen-8-yl]-acetic acid methoxymethyl ester

3-amino-2-(2-aminophenyl)-4-oxo-4H-1-benzopyran-8-acetic acid methoxymethyl ester

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