Benzenesulfonothioicacid, anhydrosulfide with thiocyanic acid

Base Information

• Chemical Name: Benzenesulfonothioicacid, anhydrosulfide with thiocyanic acid
• CAS No.: 1197-98-4
• Molecular Formula: C7H5 N O2 S2
• Molecular Weight: 199.254

Synonyms:Benzenesulfonicacid, anhydride with thiocyanic acid (7CI,8CI); Thiocyanic acid, anhydride withbenzenesulfonic acid (8CI); Benzenesulfonyl thiocyanate

Chemical Property of Benzenesulfonothioicacid, anhydrosulfide with thiocyanic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenesulfonothioicacid, anhydrosulfide with thiocyanic acid

There total 2 articles about Benzenesulfonothioicacid, anhydrosulfide with thiocyanic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

thiocyanogen (505-14-6) + sodium benzenesulfonate (873-55-2) → benzenesulfonyl thiocyanate (1197-98-4)

Guidance literature:

In water; benzene; for 1h;

Reference yield:

→ benzenesulfonyl thiocyanate (1197-98-4)

Guidance literature:

Pb(SCN)2, 1) Brom (-> (SCN)2), 2) Na-Benzolsulfinat;

Reference yield: 75.0%

benzenesulfonyl thiocyanate (1197-98-4) + isoprene (78-79-5,9003-31-0) → 1-(p-tolylsulfonyl)-4-thiocyanato-2-methyl-2-butene (80120-60-1)

Guidance literature:

In benzene; at 40 ℃; for 6h;

upstream raw materials:

thiocyanogen

sodium benzenesulfonate

Downstream raw materials:

((E)-4-Thiocyanato-pent-2-ene-1-sulfonyl)-benzene

((E)-5,5-Dimethyl-4-thiocyanato-hex-2-ene-1-sulfonyl)-benzene

1-(phenylsulfonyl)-4-thiocynato-2-butene

1-(p-tolylsulfonyl)-4-thiocyanato-2-methyl-2-butene

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