Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl methyl ester

Base Information

Chemical Name:Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl methyl ester
CAS No.:599173-45-2
Molecular Formula:C27H37N3O9S
Molecular Weight:579.671
Hs Code.:

Carbonic acid,
(1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4-
nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl methyl ester

Synonyms:

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Chemical Property of Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl methyl ester

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

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Technology Process of Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl methyl ester

There total 1 articles about Carbonic acid, (1R,2S)-2-[[(1,1-dimethylethoxy)carbonyl]amino]-1-[[(2-methylpropyl)[(4- nitrophenyl)sulfonyl]amino]methyl]-3-phenylpropyl methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 79-22-1
methyl chloroformate

: 191226-98-9
[(1S,2R)-3-[(4-nitrophenylsulfonyl)(2-methylpropyl)amino]-2-hydroxy-1-(phenylmethyl)propyl]carbamic acid tert-butyl ester

: 599173-45-2
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester methyl ester

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at 0 - 20 ℃; for 3h;
DOI:10.1016/S0960-894X(03)00463-3

Reference yield:

: 599173-45-2
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester methyl ester

: N-(4-benzyl-2-oxo-oxazolidin-5-ylmethyl)-N-isobutyl-4-nitro-benzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.33 h / 20 °C

2: aq. phosphate buffer / tetrahydrofuran / 20 °C / pH 7.0

With phosphate buffer; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0960-894X(03)00463-3

Reference yield:

: 599173-45-2
Carbonic acid (1R,2S)-2-tert-butoxycarbonylamino-1-{[isobutyl-(4-nitro-benzenesulfonyl)-amino]-methyl}-3-phenyl-propyl ester methyl ester

: {(1S,2R)-1-Benzyl-2-hydroxy-3-[isobutyl-(4-nitro-benzenesulfonyl)-amino]-propyl}-carbamic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: CH₂Cl₂ / 0.33 h / 20 °C

2: 4 mg / aq. phosphate buffer / tetrahydrofuran / 20 °C / pH 7.0

With phosphate buffer; In tetrahydrofuran; dichloromethane;
DOI:10.1016/S0960-894X(03)00463-3