11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate

Base Information

Chemical Name:11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate
CAS No.:84964-55-6
Molecular Formula:C₄H₄O₄*C₂₅H₂₇NS
Molecular Weight:489.635
Hs Code.:

Synonyms:11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate;84964-55-6;Dibenzo(b,e)thiepin-11-propanamine, 6,11-dihydro-N,N-dimethyl-11-phenyl-, (Z)-2-butenedioate (1:1)

Suppliers and Price of 11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate

Chemical Property:

Vapor Pressure:2.1E-09mmHg at 25°C
Boiling Point:480.8°Cat760mmHg
Flash Point:244.6°C
Density:g/cm³
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:6
Exact Mass:489.19737964
Heavy Atom Count:35
Complexity:587

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C[NH+](C)CCCC1(C2=CC=CC=C2CSC3=CC=CC=C31)C4=CC=CC=C4.C(=CC(=O)[O-])C(=O)O
Isomeric SMILES:C[NH+](C)CCCC1(C2=CC=CC=C2CSC3=CC=CC=C31)C4=CC=CC=C4.C(=C\C(=O)[O-])\C(=O)O

Technology Process of 11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate

There total 4 articles about 11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzo(b,e)thiepin hydrogen maleate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-86-1,52753-63-6
bromobenzene

: 84964-55-6
11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzothiepin hydrogen maleate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 1) ether, reflux; ether/benzene, reflux, 4 h

2: 91 percent / SOCl₂ / CH₂Cl₂ / 3 h / Heating

3: Mg / 1) Ether, reflux, 5 h; 2) ether/benzene, reflux, 3.5 h

With thionyl chloride; magnesium; In dichloromethane;
DOI:10.1135/cccc19823094

Reference yield:

: 68276-30-2
11-Phenyl-6,11-dihydrodibenzothiepin-11-ol

: 84964-55-6
11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzothiepin hydrogen maleate

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / SOCl₂ / CH₂Cl₂ / 3 h / Heating

2: Mg / 1) Ether, reflux, 5 h; 2) ether/benzene, reflux, 3.5 h

With thionyl chloride; magnesium; In dichloromethane;
DOI:10.1135/cccc19823094

Reference yield:

: 1531-77-7
dibenzo[b,e]thiepin-11(6H)-one

: 84964-55-6
11-(3-Dimethylaminopropyl)-11-phenyl-6,11-dihydrodibenzothiepin hydrogen maleate

Guidance literature:: Multi-step reaction with 3 steps

1: 1) Mg / 1) ether, reflux; ether/benzene, reflux, 4 h

2: 91 percent / SOCl₂ / CH₂Cl₂ / 3 h / Heating

3: Mg / 1) Ether, reflux, 5 h; 2) ether/benzene, reflux, 3.5 h

With thionyl chloride; magnesium; In dichloromethane;
DOI:10.1135/cccc19823094